S-methyl O-<(2R,3S,6S)-2-methyl-6-propyl-N-tosylpiperidin-3-yl> dithiocarbonate

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Chemical Name:S-methyl O-<(2R,3S,6S)-2-methyl-6-propyl-N-tosylpiperidin-3-yl> dithiocarbonate
CAS No.:148256-98-8
Molecular Formula:C₁₈H₂₇NO₃S₃
Molecular Weight:401.615
Hs Code.:

Synonyms:S-methyl O-<(2R,3S,6S)-2-methyl-6-propyl-N-tosylpiperidin-3-yl> dithiocarbonate

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Chemical Property of S-methyl O-<(2R,3S,6S)-2-methyl-6-propyl-N-tosylpiperidin-3-yl> dithiocarbonate

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Technology Process of S-methyl O-<(2R,3S,6S)-2-methyl-6-propyl-N-tosylpiperidin-3-yl> dithiocarbonate

There total 5 articles about S-methyl O-<(2R,3S,6S)-2-methyl-6-propyl-N-tosylpiperidin-3-yl> dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 148346-40-1
(2R,6R)-1,6-dihydro-6-hydroxy-2-methyl-N-tosylpyridin-3(2H)-one

: 148256-98-8
S-methyl O-<(2R,3S,6S)-2-methyl-6-propyl-N-tosylpiperidin-3-yl> dithiocarbonate

Guidance literature:: Multi-step reaction with 5 steps

1: 99.8 percent / BF₃*Et₂O, 4 Angstroem molecular sieves / diethyl ether / 2 h / Ambient temperature

2: 90 percent / NaBH₄ / methanol / 0.33 h / -60 - -20 °C

3: 79.2 percent / TiCl₄ / CH₂Cl₂ / 2 h / -70 - 0 °C

4: 100 percent / H₂ / 10percent Pd/C / ethanol / 24 h / 760 Torr / Ambient temperature

5: 1) NaH, imidazole / 1) THF, reflux, 30 min, 2) reflux, 30 min

With 1H-imidazole; sodium tetrahydroborate; 4 A molecular sieve; boron trifluoride diethyl etherate; hydrogen; titanium tetrachloride; sodium hydride; palladium on activated charcoal; In methanol; diethyl ether; ethanol; dichloromethane;

Reference yield:

: 148256-94-4
(2R,3S,6R)-6-allyl-2-methyl-N-tosylpiperidin-3-ol

: 148256-98-8
S-methyl O-<(2R,3S,6S)-2-methyl-6-propyl-N-tosylpiperidin-3-yl> dithiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / 10percent Pd/C / ethanol / 24 h / 760 Torr / Ambient temperature

2: 1) NaH, imidazole / 1) THF, reflux, 30 min, 2) reflux, 30 min

With 1H-imidazole; hydrogen; sodium hydride; palladium on activated charcoal; In ethanol;

Reference yield:

: 148256-92-2
(2R,6R)-6-ethoxy-1,6-dihydro-2-methyl-N-tosylpyridin-3(2H)-one

: 148256-98-8
S-methyl O-<(2R,3S,6S)-2-methyl-6-propyl-N-tosylpiperidin-3-yl> dithiocarbonate

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / NaBH₄ / methanol / 0.33 h / -60 - -20 °C

2: 79.2 percent / TiCl₄ / CH₂Cl₂ / 2 h / -70 - 0 °C

3: 100 percent / H₂ / 10percent Pd/C / ethanol / 24 h / 760 Torr / Ambient temperature

4: 1) NaH, imidazole / 1) THF, reflux, 30 min, 2) reflux, 30 min

With 1H-imidazole; sodium tetrahydroborate; hydrogen; titanium tetrachloride; sodium hydride; palladium on activated charcoal; In methanol; ethanol; dichloromethane;