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Technology Process of C52H73ClO9SSi

C52H73ClO9SSi

Base Information
  • Chemical Name:C52H73ClO9SSi
  • CAS No.:1193376-94-1
  • Molecular Formula:C52H73ClO9SSi
  • Molecular Weight:937.751
  • Hs Code.:
C<sub>52</sub>H<sub>73</sub>ClO<sub>9</sub>SSi

Synonyms:C52H73ClO9SSi

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Chemical Property of C52H73ClO9SSi
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Technology Process of C52H73ClO9SSi

There total 1 articles about C52H73ClO9SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-((2S,3S,4R,5R)-5-(((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl)-4-methoxy-3-((phenylsulfonyl)methyl)tetrahydrofuran-2-yl)acetaldehyde

2-((2S,3S,4R,5R)-5-(((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl)-4-methoxy-3-((phenylsulfonyl)methyl)tetrahydrofuran-2-yl)acetaldehyde

C<sub>32</sub>H<sub>44</sub>ClIO<sub>2</sub>Si
1193376-88-3

C32H44ClIO2Si

C<sub>52</sub>H<sub>73</sub>ClO<sub>9</sub>SSi
1193376-94-1

C52H73ClO9SSi

Guidance literature:
With chromium dichloride; manganese; zirconocene dichloride; 2.9-dimethyl-1,10-phenanthroline; N-(2-((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)-6-(((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl)oxy)phenyl)benzenesulfonamide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; lithium chloride; In acetonitrile; at 20 ℃; for 6h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ja9058475

Reference yield: 84.0%

C<sub>52</sub>H<sub>73</sub>ClO<sub>9</sub>SSi
1193376-94-1

C52H73ClO9SSi

C<sub>52</sub>H<sub>72</sub>O<sub>9</sub>SSi
1193376-97-4

C52H72O9SSi

Guidance literature:
With silver tetrafluoroborate; 2,6-di-tert-butyl-4-methylpyridine; In acetic acid tert-butyl ester; at 0 - 20 ℃; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ja9058475
upstream raw materials:

C32H44ClIO2Si

Downstream raw materials:

C52H72O9SSi

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