bisfurfuryl 4,4'-[(2,5-dibromo-1,4-phenylene)bisoxy]dibutanoate

Base Information

Chemical Name:bisfurfuryl 4,4'-[(2,5-dibromo-1,4-phenylene)bisoxy]dibutanoate
CAS No.:1206606-84-9
Molecular Formula:C₂₄H₂₄Br₂O₈
Molecular Weight:600.258
Hs Code.:

Synonyms:bisfurfuryl 4,4'-[(2,5-dibromo-1,4-phenylene)bisoxy]dibutanoate

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Chemical Property of bisfurfuryl 4,4'-[(2,5-dibromo-1,4-phenylene)bisoxy]dibutanoate

Chemical Property:

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Technology Process of bisfurfuryl 4,4'-[(2,5-dibromo-1,4-phenylene)bisoxy]dibutanoate

There total 2 articles about bisfurfuryl 4,4'-[(2,5-dibromo-1,4-phenylene)bisoxy]dibutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1206606-83-8
furfuryl 4-chlorobutanoate

: 14753-51-6
2,5-dibromohydroquinone

: 1206606-84-9
bisfurfuryl 4,4'-[(2,5-dibromo-1,4-phenylene)bisoxy]dibutanoate

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 140 ℃; for 2.5h;
DOI:10.1021/ma902180r

Reference yield:

: 98-00-0,25212-86-6,93793-62-5
(2-furyl)methyl alcohol

: 1206606-84-9
bisfurfuryl 4,4'-[(2,5-dibromo-1,4-phenylene)bisoxy]dibutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Cooling with ice

2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 2.5 h / 140 °C

With potassium carbonate; triethylamine; potassium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ma902180r

Reference yield:

: 1206606-84-9
bisfurfuryl 4,4'-[(2,5-dibromo-1,4-phenylene)bisoxy]dibutanoate

: 1066-54-2
trimethylsilylacetylene

: C₃₄H₄₂O₈Si₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide; at 55 ℃; for 16h;
DOI:10.1021/ma902180r