octyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-glucopyranoside

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Chemical Name:octyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-glucopyranoside
CAS No.:368870-55-7
Molecular Formula:C₄₉H₅₇NO₆
Molecular Weight:755.995
Hs Code.:

Synonyms:octyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-glucopyranoside

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Chemical Property of octyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-glucopyranoside

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Technology Process of octyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-glucopyranoside

There total 4 articles about octyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 100-39-0
benzyl bromide

: 368870-54-6
octyl 2-acetamido-2-deoxy-6-O-trityl-α-D-glucopyranoside

: 368870-55-7
octyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-glucopyranoside

Guidance literature:: octyl 2-acetamido-2-deoxy-6-O-trityl-α-D-glucopyranoside; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.166667h;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; at 80 ℃; for 1.5h;
DOI:10.1021/jm025620k

Reference yield:

: 111-87-5
octanol

: 368870-55-7
octyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 42 percent / BF₃*Et₂O / nitromethane / 100 °C

2.1: 84 percent / DMAP; pyridine / 4.5 h / 100 °C

3.1: NaH / tetrahydrofuran / 0.17 h / 0 °C

3.2: 89 percent / tetrabutylammonium iodide / tetrahydrofuran / 1.5 h / 80 °C

With pyridine; dmap; boron trifluoride diethyl etherate; sodium hydride; In tetrahydrofuran; nitromethane;
DOI:10.1021/jm025620k

Reference yield:

: 7512-17-6,72-87-7,1136-42-1,1136-44-3,6082-29-7,6730-06-9,7772-94-3,10036-64-3,14131-60-3,14131-64-7,14131-68-1,14215-68-0,62057-49-2,62057-50-5,62057-51-6,62057-52-7,62057-53-8,62057-54-9,62057-55-0,62057-56-1,62075-50-7,62137-54-6,134451-97-1,134522-12-6,148347-16-4
N-Acetyl-D-glucosamine

: 368870-55-7
octyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 42 percent / BF₃*Et₂O / nitromethane / 100 °C

2.1: 84 percent / DMAP; pyridine / 4.5 h / 100 °C

3.1: NaH / tetrahydrofuran / 0.17 h / 0 °C

3.2: 89 percent / tetrabutylammonium iodide / tetrahydrofuran / 1.5 h / 80 °C

With pyridine; dmap; boron trifluoride diethyl etherate; sodium hydride; In tetrahydrofuran; nitromethane;
DOI:10.1021/jm025620k