C₃₄H₄₆ClN₃O₇

Base Information

Chemical Name:C₃₄H₄₆ClN₃O₇
CAS No.:1009093-39-3
Molecular Formula:C₃₄H₄₆ClN₃O₇
Molecular Weight:644.208
Hs Code.:

C<sub>34</sub>H<sub>46</sub>ClN<sub>3</sub>O<sub>7</sub>

Synonyms:C₃₄H₄₆ClN₃O₇

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Chemical Property of C₃₄H₄₆ClN₃O₇

Chemical Property:

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Technology Process of C₃₄H₄₆ClN₃O₇

There total 14 articles about C₃₄H₄₆ClN₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1009094-76-1
C₃₂H₄₂ClN₃O₇

: 1009093-39-3
C₃₄H₄₆ClN₃O₇

Guidance literature:: With sodium cyanoborohydride; In methanol; water; at 20 ℃; for 0.5h;

Reference yield:

: 3-bromo-6-fluoro-2-hydroxybenzaldehyde

: 1009093-39-3
C₃₄H₄₆ClN₃O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 40 °C

2.1: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C

3.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2

4.1: toluene / 14 h / Heating / reflux

5.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C

6.1: trimethylaluminum / hexanes; dichloromethane / 0.33 h

6.2: 20 °C

6.3: 15 h / 20 °C

7.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 24 h / 60 °C

8.1: sodium cyanoborohydride / methanol; water / 0.5 h / 20 °C

With hydrogenchloride; hydroxylamine hydrochloride; methyl orange; trimethylaluminum; potassium acetate; sodium cyanoborohydride; potassium carbonate; caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; hexanes; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 473416-74-9
3-bromo-6-fluoro-2-methoxybenzaldehyde

: 1009093-39-3
C₃₄H₄₆ClN₃O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C

2.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2

3.1: toluene / 14 h / Heating / reflux

4.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C

5.1: trimethylaluminum / hexanes; dichloromethane / 0.33 h

5.2: 20 °C

5.3: 15 h / 20 °C

6.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 24 h / 60 °C

7.1: sodium cyanoborohydride / methanol; water / 0.5 h / 20 °C

With hydrogenchloride; hydroxylamine hydrochloride; methyl orange; trimethylaluminum; potassium acetate; sodium cyanoborohydride; caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; hexanes; dichloromethane; water; dimethyl sulfoxide; toluene;