7-O-p-chlorobenzyl-25-O-methyl-26-O-t-butyldimethylsilylmonensin methyl ester

Base Information

Chemical Name:7-O-p-chlorobenzyl-25-O-methyl-26-O-t-butyldimethylsilylmonensin methyl ester
CAS No.:346694-31-3
Molecular Formula:C₅₁H₈₅ClO₁₁Si
Molecular Weight:937.768
Hs Code.:

Synonyms:7-O-p-chlorobenzyl-25-O-methyl-26-O-t-butyldimethylsilylmonensin methyl ester

Suppliers and Price of 7-O-p-chlorobenzyl-25-O-methyl-26-O-t-butyldimethylsilylmonensin methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-O-p-chlorobenzyl-25-O-methyl-26-O-t-butyldimethylsilylmonensin methyl ester

Chemical Property:

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Technology Process of 7-O-p-chlorobenzyl-25-O-methyl-26-O-t-butyldimethylsilylmonensin methyl ester

There total 4 articles about 7-O-p-chlorobenzyl-25-O-methyl-26-O-t-butyldimethylsilylmonensin methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 622-95-7
4-chlorobenzyl bromide

: 244088-32-2
25-O-methyl-26-O-t-butyldimethylsilylmonensin methyl ester

: 346694-31-3
7-O-p-chlorobenzyl-25-O-methyl-26-O-t-butyldimethylsilylmonensin methyl ester

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/S0040-4020(01)00154-5

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 346694-31-3
7-O-p-chlorobenzyl-25-O-methyl-26-O-t-butyldimethylsilylmonensin methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / imidazole / tetrahydrofuran / 22 h / 20 °C

2: 50 percent / sodium hydride; tetra-n-butylammonium iodide / tetrahydrofuran / 20 °C

With 1H-imidazole; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)00154-5

Reference yield:

: 116278-62-7
25-O-methylmonensin methyl ester

: 346694-31-3
7-O-p-chlorobenzyl-25-O-methyl-26-O-t-butyldimethylsilylmonensin methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / imidazole / tetrahydrofuran / 22 h / 20 °C

2: 50 percent / sodium hydride; tetra-n-butylammonium iodide / tetrahydrofuran / 20 °C

With 1H-imidazole; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)00154-5