C₂₀H₁₃F₅N₂O₃

Base Information

Chemical Name:C₂₀H₁₃F₅N₂O₃
CAS No.:1276039-92-9
Molecular Formula:C₂₀H₁₃F₅N₂O₃
Molecular Weight:424.327
Hs Code.:

C<sub>20</sub>H<sub>13</sub>F<sub>5</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₀H₁₃F₅N₂O₃

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Chemical Property of C₂₀H₁₃F₅N₂O₃

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Technology Process of C₂₀H₁₃F₅N₂O₃

There total 5 articles about C₂₀H₁₃F₅N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1276039-91-8
C₂₁H₁₅F₅N₂O₃

: 1276039-92-9
C₂₀H₁₃F₅N₂O₃

Guidance literature:: C₂₁H₁₅F₅N₂O₃; With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃;

With hydrogenchloride; In tetrahydrofuran; methanol; water; pH=5.5;

Reference yield:

: 40263-57-8
2-iodo-3-hydroxypyridine

: 1276039-92-9
C₂₀H₁₃F₅N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium fluoride; copper(l) iodide / 1-methyl-pyrrolidin-2-one / 120 °C / Inert atmosphere

2.1: caesium carbonate / dimethyl sulfoxide / 2 h / 70 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol / 4 h

4.1: sodium tris(acetoxy)borohydride; sodium cyanoborohydride; acetic acid / 1,2-dichloro-ethane / 20 °C

5.1: water; sodium hydroxide / tetrahydrofuran; methanol / 20 °C

5.2: pH 5.5

With potassium fluoride; copper(l) iodide; water; hydrogen; sodium tris(acetoxy)borohydride; sodium cyanoborohydride; caesium carbonate; acetic acid; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dimethyl sulfoxide; 1,2-dichloro-ethane;

Reference yield:

: 1063697-17-5
3-hydroxy-2-trifluoromethylpyridine

: 1276039-92-9
C₂₀H₁₃F₅N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / dimethyl sulfoxide / 2 h / 70 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol / 4 h

3.1: sodium tris(acetoxy)borohydride; sodium cyanoborohydride; acetic acid / 1,2-dichloro-ethane / 20 °C

4.1: water; sodium hydroxide / tetrahydrofuran; methanol / 20 °C

4.2: pH 5.5

With water; hydrogen; sodium tris(acetoxy)borohydride; sodium cyanoborohydride; caesium carbonate; acetic acid; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dimethyl sulfoxide; 1,2-dichloro-ethane;