C₂₂H₁₆O

Base Information

• Chemical Name: C₂₂H₁₆O
• CAS No.: 1606161-44-7
• Molecular Formula: C₂₂H₁₆O
• Molecular Weight: 296.368
• Mol file: 1606161-44-7.mol

Synonyms:C₂₂H₁₆O

Chemical Property of C₂₂H₁₆O

Chemical Property:

Purity/Quality:

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Technology Process of C₂₂H₁₆O

There total 1 articles about C₂₂H₁₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-ethynyl-1,1'-biphenyl (29079-00-3) + 2-bromophenyl methyl ketone (2142-69-0) → C22H16O (1606161-44-7)

Guidance literature:

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine; In tetrahydrofuran; at 90 ℃; for 24h; Inert atmosphere;

DOI:10.1021/jo500182k

Reference yield: 58.0%

C22H16O (1606161-44-7) → 12-methyl-5-(4-phenylphenyl)-6-(4-phenylbenzoyl)chrysene (1606161-31-2)

Guidance literature:

With triethylamine; orthoformic acid triethyl ester; copper dichloride; In 1,4-dioxane; at 120 ℃; for 12h;

DOI:10.1021/jo500182k

upstream raw materials:

4-ethynyl-1,1'-biphenyl

2-bromophenyl methyl ketone

Downstream raw materials:

12-methyl-5-(4-phenylphenyl)-6-(4-phenylbenzoyl)chrysene