2-{[4-cyano-5-(methylsulfanyl)-1,2-thiazol-3-yl]sulfanyl}acetamide

Base Information

• Chemical Name: 2-{[4-cyano-5-(methylsulfanyl)-1,2-thiazol-3-yl]sulfanyl}acetamide
• CAS No.: 24134-92-7
• Molecular Formula: C₇H₇N₃OS₃
• Molecular Weight: 245.35
• Mol file: 24134-92-7.mol

Synonyms:Acetamide,2-[(4-cyano-5-(methylthio)-3-isothiazolyl)thio]- (8CI,9CI)

Chemical Property of 2-{[4-cyano-5-(methylsulfanyl)-1,2-thiazol-3-yl]sulfanyl}acetamide

Chemical Property:

• Vapor Pressure: 1.04E-05mmHg at 25°C
• Boiling Point: 371.4°C at 760 mmHg
• Flash Point: 178.4°C
• Density: 1.52g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-{[4-cyano-5-(methylsulfanyl)-1,2-thiazol-3-yl]sulfanyl}acetamide

There total 1 articles about 2-{[4-cyano-5-(methylsulfanyl)-1,2-thiazol-3-yl]sulfanyl}acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-bis(sodiomercapto)isothiazole-4-carbonitrile (2076-67-7) + dimethyl sulfate (77-78-1) + Chloroacetamide (79-07-2) → 2-(4-Cyano-5-methylsulfanyl-isothiazol-3-ylsulfanyl)-acetamide (24134-92-7)

Guidance literature:

Yield given. Multistep reaction; 1) MeOH, 1 h, room temp; 2) MeOH, water, 1 h;

Reference yield: 85.0%

2-(4-Cyano-5-methylsulfanyl-isothiazol-3-ylsulfanyl)-acetamide (24134-92-7) → 4-Amino-3-methylsulfanyl-thieno[2,3-c]isothiazole-5-carboxylic acid amide (77726-64-8)

Guidance literature:

With sodium methylate; In methanol; for 0.5h;

upstream raw materials:

3,5-bis(sodiomercapto)isothiazole-4-carbonitrile

dimethyl sulfate

Chloroacetamide

Downstream raw materials:

4-Amino-3-methylsulfanyl-thieno[2,3-c]isothiazole-5-carboxylic acid amide

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