ethyl 4-methoxy-3-(N-(2-morpholinoethyl)-methylsulfonamido)phenyl carbonate?

Base Information

Chemical Name:ethyl 4-methoxy-3-(N-(2-morpholinoethyl)-methylsulfonamido)phenyl carbonate?
CAS No.:1428848-01-4
Molecular Formula:C₁₇H₂₆N₂O₇S
Molecular Weight:402.469
Hs Code.:

Synonyms:ethyl 4-methoxy-3-(N-(2-morpholinoethyl)-methylsulfonamido)phenyl carbonate?

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Chemical Property of ethyl 4-methoxy-3-(N-(2-morpholinoethyl)-methylsulfonamido)phenyl carbonate?

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Technology Process of ethyl 4-methoxy-3-(N-(2-morpholinoethyl)-methylsulfonamido)phenyl carbonate?

There total 5 articles about ethyl 4-methoxy-3-(N-(2-morpholinoethyl)-methylsulfonamido)phenyl carbonate? which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.14%

: 1428848-00-3
ethyl 4-methoxy-3-(methylsulfonamido)phenyl carbonate

: 3647-69-6
4-(2-chloroethyl)morpholine hydrochride

: 1428848-01-4
ethyl 4-methoxy-3-(N-(2-morpholinoethyl)-methylsulfonamido)phenyl carbonate?

Guidance literature:: ethyl 4-methoxy-3-(methylsulfonamido)phenyl carbonate; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.166667h; Inert atmosphere;

4-(2-chloroethyl)morpholine hydrochride; In N,N-dimethyl-formamide; at 90 ℃; for 2h;

Reference yield:

: ethyl 4-methoxy-3-nitrophenyl carbonate

: 1428848-01-4
ethyl 4-methoxy-3-(N-(2-morpholinoethyl)-methylsulfonamido)phenyl carbonate?

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium 10% on activated carbon; hydrogen; acetic acid / ethyl acetate / 2 h / 1292.9 Torr

2.1: pyridine / dichloromethane / 3 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

3.2: 2 h / 90 °C

With pyridine; palladium 10% on activated carbon; hydrogen; sodium hydride; acetic acid; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 98083-21-7
3-amino-4-methoxyphenyl ethyl carbonate

: 1428848-01-4
ethyl 4-methoxy-3-(N-(2-morpholinoethyl)-methylsulfonamido)phenyl carbonate?

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 3 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

2.2: 2 h / 90 °C

With pyridine; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;