1-(3,3-dimethyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)but-1-en-2-yl)-4-methoxybenzene

Base Information

Chemical Name:1-(3,3-dimethyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)but-1-en-2-yl)-4-methoxybenzene
CAS No.:1642593-57-4
Molecular Formula:C₂₂H₃₂O
Molecular Weight:312.495
Hs Code.:

Synonyms:1-(3,3-dimethyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)but-1-en-2-yl)-4-methoxybenzene

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Chemical Property of 1-(3,3-dimethyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)but-1-en-2-yl)-4-methoxybenzene

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Technology Process of 1-(3,3-dimethyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)but-1-en-2-yl)-4-methoxybenzene

There total 3 articles about 1-(3,3-dimethyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)but-1-en-2-yl)-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1642593-76-7
C₂₁H₃₀O₂

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1642593-57-4
1-(3,3-dimethyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)but-1-en-2-yl)-4-methoxybenzene

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

C₂₁H₃₀O₂; In tetrahydrofuran; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.3762/bjoc.10.128

Reference yield:

: 59633-88-4
2-(bromomethyl)-1,3,3-trimethylcyclohex-1-ene

: 1642593-57-4
1-(3,3-dimethyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)but-1-en-2-yl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: 16 h / 0 - 20 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2.2: 16 h / 0 - 20 °C / Inert atmosphere

With potassium tert-butylate; In tetrahydrofuran; 2.1: |Wittig Olefination / 2.2: |Wittig Olefination;
DOI:10.3762/bjoc.10.128

Reference yield:

: 2040-20-2
4-methoxyisobutyrophenone

: 1642593-57-4
1-(3,3-dimethyl-4-(2,6,6-trimethylcyclohex-1-en-1-yl)but-1-en-2-yl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: 16 h / 0 - 20 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2.2: 16 h / 0 - 20 °C / Inert atmosphere

With potassium tert-butylate; In tetrahydrofuran; 2.1: |Wittig Olefination / 2.2: |Wittig Olefination;
DOI:10.3762/bjoc.10.128