(1S,4aS,5S,8aS)-5-(3,5-Dimethoxy-benzyl)-5,8a-dimethyl-6-methylene-decahydro-naphthalen-1-ol

Base Information

Chemical Name:(1S,4aS,5S,8aS)-5-(3,5-Dimethoxy-benzyl)-5,8a-dimethyl-6-methylene-decahydro-naphthalen-1-ol
CAS No.:188477-52-3
Molecular Formula:C₂₂H₃₂O₃
Molecular Weight:344.494
Hs Code.:

Synonyms:(1S,4aS,5S,8aS)-5-(3,5-Dimethoxy-benzyl)-5,8a-dimethyl-6-methylene-decahydro-naphthalen-1-ol

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Chemical Property of (1S,4aS,5S,8aS)-5-(3,5-Dimethoxy-benzyl)-5,8a-dimethyl-6-methylene-decahydro-naphthalen-1-ol

Chemical Property:

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Technology Process of (1S,4aS,5S,8aS)-5-(3,5-Dimethoxy-benzyl)-5,8a-dimethyl-6-methylene-decahydro-naphthalen-1-ol

There total 3 articles about (1S,4aS,5S,8aS)-5-(3,5-Dimethoxy-benzyl)-5,8a-dimethyl-6-methylene-decahydro-naphthalen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 877-88-3
3,5-dimethoxybenzyl bromide

: 188477-52-3
(1S,4aS,5S,8aS)-5-(3,5-Dimethoxy-benzyl)-5,8a-dimethyl-6-methylene-decahydro-naphthalen-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Li, NH₃ / 1) THF, reflux, 30 min; 2) THF, 30 min, rt

2: 1.) NaH, DMSO / 1) 25 deg C, 1 h; 2) 75 deg C, 4 h

With ammonia; lithium; sodium hydride; dimethyl sulfoxide;
DOI:10.1021/jo962292l

Reference yield:

: 38405-15-1
(4aS,5S)-4,4a,5,6,7,8-hexahydro-5-hydroxy-1,4a-dimethylnaphthalen-2(3H)-one

: 188477-52-3
(1S,4aS,5S,8aS)-5-(3,5-Dimethoxy-benzyl)-5,8a-dimethyl-6-methylene-decahydro-naphthalen-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Li, NH₃ / 1) THF, reflux, 30 min; 2) THF, 30 min, rt

2: 1.) NaH, DMSO / 1) 25 deg C, 1 h; 2) 75 deg C, 4 h

With ammonia; lithium; sodium hydride; dimethyl sulfoxide;
DOI:10.1021/jo962292l

Reference yield:

: 1779-49-3
Methyltriphenylphosphonium bromide

: 188477-51-2
(1S,4aS,5S,8aR)-1-(3,5-Dimethoxy-benzyl)-5-hydroxy-1,4a-dimethyl-octahydro-naphthalen-2-one

: 188477-52-3
(1S,4aS,5S,8aS)-5-(3,5-Dimethoxy-benzyl)-5,8a-dimethyl-6-methylene-decahydro-naphthalen-1-ol

Guidance literature:: With sodium hydride; dimethyl sulfoxide; Yield given. Multistep reaction; 1) 25 deg C, 1 h; 2) 75 deg C, 4 h;
DOI:10.1021/jo962292l