2-(2,2-diphenyl-benzo[1,3]dioxol-5-yl)-3,5-bisbenzyloxy-7-β-D-glucopyranosyloxy-4H-chromen-4-one

Base Information

Chemical Name:2-(2,2-diphenyl-benzo[1,3]dioxol-5-yl)-3,5-bisbenzyloxy-7-β-D-glucopyranosyloxy-4H-chromen-4-one
CAS No.:1313191-79-5
Molecular Formula:C₄₈H₄₀O₁₂
Molecular Weight:808.838
Hs Code.:

Synonyms:2-(2,2-diphenyl-benzo[1,3]dioxol-5-yl)-3,5-bisbenzyloxy-7-β-D-glucopyranosyloxy-4H-chromen-4-one

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Chemical Property of 2-(2,2-diphenyl-benzo[1,3]dioxol-5-yl)-3,5-bisbenzyloxy-7-β-D-glucopyranosyloxy-4H-chromen-4-one

Chemical Property:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(2,2-diphenyl-benzo[1,3]dioxol-5-yl)-3,5-bisbenzyloxy-7-β-D-glucopyranosyloxy-4H-chromen-4-one

There total 6 articles about 2-(2,2-diphenyl-benzo[1,3]dioxol-5-yl)-3,5-bisbenzyloxy-7-β-D-glucopyranosyloxy-4H-chromen-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1313191-78-4
2-(2,2-diphenyl-benzo[1,3]dioxol-5-yl)-3,5-bisbenzyloxy-7-(2,3,4,6-tetra-O-acetyl)-β-D-glucopyranosyloxy-4H-chromen-4-one

: 1313191-79-5
2-(2,2-diphenyl-benzo[1,3]dioxol-5-yl)-3,5-bisbenzyloxy-7-β-D-glucopyranosyloxy-4H-chromen-4-one

Guidance literature:: 2-(2,2-diphenyl-benzo[1,3]dioxol-5-yl)-3,5-bisbenzyloxy-7-(2,3,4,6-tetra-O-acetyl)-β-D-glucopyranosyloxy-4H-chromen-4-one; With sodium methylate; In tetrahydrofuran; methanol; at 20 ℃;

In tetrahydrofuran; methanol; for 0.5h;
DOI:10.1016/j.tet.2011.03.110

Reference yield:

: 2051-90-3
Dichlorodiphenylmethane

: 1313191-79-5
2-(2,2-diphenyl-benzo[1,3]dioxol-5-yl)-3,5-bisbenzyloxy-7-β-D-glucopyranosyloxy-4H-chromen-4-one

Guidance literature:: Multi-step reaction with 5 steps

1.1: 0.17 h / 180 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

3.1: Tris(3,6-dioxaheptyl)amine; potassium carbonate / dichloromethane; water / 24 h / Inert atmosphere

4.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

5.1: sodium methylate / tetrahydrofuran; methanol / 20 °C

5.2: ion-exchange resin / 0.5 h

With Tris(3,6-dioxaheptyl)amine; sodium methylate; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.03.110

Reference yield:

: 1313191-77-3
2-(2,2-diphenyl-benzo[1,3]dioxol-5-yl)-3-benzyloxy-5-hydroxyl-7-(2,3,4,6-tetra-O-acetyl)-β-D-glucopyranosyloxy-4H-chromen-4-one

: 1313191-79-5
2-(2,2-diphenyl-benzo[1,3]dioxol-5-yl)-3,5-bisbenzyloxy-7-β-D-glucopyranosyloxy-4H-chromen-4-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

2.1: sodium methylate / tetrahydrofuran; methanol / 20 °C

2.2: ion-exchange resin / 0.5 h

With sodium methylate; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.03.110