dl-trans-2-<2-<(phenylsulfonyl)amino>cyclopent-4-enyl>ethanol triphenylmethyl ether

Base Information

Chemical Name:dl-trans-2-<2-<(phenylsulfonyl)amino>cyclopent-4-enyl>ethanol triphenylmethyl ether
CAS No.:113007-90-2
Molecular Formula:C₃₂H₃₁NO₃S
Molecular Weight:509.669
Hs Code.:

Synonyms:dl-trans-2-<2-<(phenylsulfonyl)amino>cyclopent-4-enyl>ethanol triphenylmethyl ether

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Chemical Property of dl-trans-2-<2-<(phenylsulfonyl)amino>cyclopent-4-enyl>ethanol triphenylmethyl ether

Chemical Property:

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Technology Process of dl-trans-2-<2-<(phenylsulfonyl)amino>cyclopent-4-enyl>ethanol triphenylmethyl ether

There total 5 articles about dl-trans-2-<2-<(phenylsulfonyl)amino>cyclopent-4-enyl>ethanol triphenylmethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113007-89-9
dl-trans-2-(2-aminocyclopent-4-enyl)ethanol triphenylmethyl ether

: 98-09-9
benzenesulfonyl chloride

: 113007-90-2
dl-trans-2-<2-<(phenylsulfonyl)amino>cyclopent-4-enyl>ethanol triphenylmethyl ether

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h; Yield given;
DOI:10.1021/jm00163a038

Reference yield:

: 49826-08-6,54483-54-4,54483-55-5,75331-67-8
1-hydroxy-2-(2-hydroxyethyl)cyclopent-3-ene

: 113007-90-2
dl-trans-2-<2-<(phenylsulfonyl)amino>cyclopent-4-enyl>ethanol triphenylmethyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / Et₃N, 4-(dimethylamino)pyridine / CH₂Cl₂ / 20 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

3: NaN₃ / dimethylformamide / 5 h / 75 °C

4: 1.) Ph₃P, 2.) H₂O / 1.) RT, 15 h, 2.) a.) 45 deg C, 2 h, b.) reflux, 1 h

5: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With dmap; sodium azide; water; triethylamine; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00163a038

Reference yield:

: 112967-36-9
dl-cis-2-(2-hydroxycyclopent-4-enyl)ethanol triphenylmethyl ether

: 113007-90-2
dl-trans-2-<2-<(phenylsulfonyl)amino>cyclopent-4-enyl>ethanol triphenylmethyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

2: NaN₃ / dimethylformamide / 5 h / 75 °C

3: 1.) Ph₃P, 2.) H₂O / 1.) RT, 15 h, 2.) a.) 45 deg C, 2 h, b.) reflux, 1 h

4: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With sodium azide; water; triethylamine; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00163a038