2-benzoylamino-5,5-dimethyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid ethyl ester

Base Information

Chemical Name:2-benzoylamino-5,5-dimethyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid ethyl ester
CAS No.:263402-83-1
Molecular Formula:C₁₉H₂₁NO₄S
Molecular Weight:359.446
Hs Code.:

2-benzoylamino-5,5-dimethyl-4,7-dihydro-5<i>H</i>-thieno[2,3-<i>c</i>]pyran-3-carboxylic acid ethyl ester

Synonyms:2-benzoylamino-5,5-dimethyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid ethyl ester

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Chemical Property of 2-benzoylamino-5,5-dimethyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid ethyl ester

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Technology Process of 2-benzoylamino-5,5-dimethyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid ethyl ester

There total 1 articles about 2-benzoylamino-5,5-dimethyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.5%

: 64792-51-4
ethyl 2-amino-5,5-dimethyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylate

: 98-88-4
benzoyl chloride

: 263402-83-1
2-benzoylamino-5,5-dimethyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid ethyl ester

Guidance literature:: With triethylamine; In benzene; for 4h; Heating;
DOI:10.1023/A:1015355729220

Reference yield: 83.1%

: 263402-83-1
2-benzoylamino-5,5-dimethyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid ethyl ester

: 263402-85-3
3-amino-6,6-dimethyl-2-phenyl-5,6-dihydro-8H-pyrano[4',3':4,5]thieno[2,3-d]pyrimidin-4-one

Guidance literature:: With hydrazine hydrate; In ethanol; for 8h; Heating;
DOI:10.1007/BF02252109

Reference yield:

: 263402-83-1
2-benzoylamino-5,5-dimethyl-4,7-dihydro-5H-thieno[2,3-c]pyran-3-carboxylic acid ethyl ester

: 6,6-Dimethyl-2-phenyl-3,5,6,8-tetrahydro-pyrano[4',3':4,5]thieno[2,3-d]pyrimidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 83.1 percent / hydrazine hydrate / ethanol / 8 h / Heating

2: 100 percent / NaNO₂ / acetic acid / 16 h / 20 °C

With hydrazine hydrate; sodium nitrite; In ethanol; acetic acid; 1: Condensation / 2: deamination;
DOI:10.1007/BF02252109