N-(methacrylamido)-1′,2,3,3′,4,4′,6-hepta-O-benzyl-6′-amino-6′-deoxysucrose

Base Information

Chemical Name:N-(methacrylamido)-1′,2,3,3′,4,4′,6-hepta-O-benzyl-6′-amino-6′-deoxysucrose
CAS No.:1613526-84-3
Molecular Formula:C₆₅H₆₉NO₁₁
Molecular Weight:1040.26
Hs Code.:

Synonyms:N-(methacrylamido)-1′,2,3,3′,4,4′,6-hepta-O-benzyl-6′-amino-6′-deoxysucrose

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Chemical Property of N-(methacrylamido)-1′,2,3,3′,4,4′,6-hepta-O-benzyl-6′-amino-6′-deoxysucrose

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Technology Process of N-(methacrylamido)-1′,2,3,3′,4,4′,6-hepta-O-benzyl-6′-amino-6′-deoxysucrose

There total 4 articles about N-(methacrylamido)-1′,2,3,3′,4,4′,6-hepta-O-benzyl-6′-amino-6′-deoxysucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1613526-83-2
1′,2,3,3′,4,4′,6-hepta-O-benzyl-6′-amino-6′-deoxysucrose

: 920-46-7,26937-45-1
Methacryloyl chloride

: 1613526-84-3
N-(methacrylamido)-1′,2,3,3′,4,4′,6-hepta-O-benzyl-6′-amino-6′-deoxysucrose

Guidance literature:: 1′,2,3,3′,4,4′,6-hepta-O-benzyl-6′-amino-6′-deoxysucrose; With dmap; triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;

Methacryloyl chloride; In dichloromethane; at 0 - 20 ℃; for 2.33333h; Inert atmosphere;
DOI:10.1016/j.carbpol.2014.03.050

Reference yield:

: 1613526-81-0
1′,2,3,3′,4,4′,6-hepta-O-benzyl-6′-O-methanesulfonylsucrose

: 1613526-84-3
N-(methacrylamido)-1′,2,3,3′,4,4′,6-hepta-O-benzyl-6′-amino-6′-deoxysucrose

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium azide / N,N-dimethyl-formamide / 0.17 h / 120 °C / Microwave irradiation

2.1: triphenylphosphine / water; tetrahydrofuran / 3 h / 70 °C

3.1: triethylamine; dmap / dichloromethane / 0 °C / Inert atmosphere

3.2: 2.33 h / 0 - 20 °C / Inert atmosphere

With dmap; sodium azide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.carbpol.2014.03.050

Reference yield:

: 103931-54-0
1,3,4-tri-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

: 1613526-84-3
N-(methacrylamido)-1′,2,3,3′,4,4′,6-hepta-O-benzyl-6′-amino-6′-deoxysucrose

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; dmap / dichloromethane / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C / Inert atmosphere

2.1: sodium azide / N,N-dimethyl-formamide / 0.17 h / 120 °C / Microwave irradiation

3.1: triphenylphosphine / water; tetrahydrofuran / 3 h / 70 °C

4.1: triethylamine; dmap / dichloromethane / 0 °C / Inert atmosphere

4.2: 2.33 h / 0 - 20 °C / Inert atmosphere

With dmap; sodium azide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.carbpol.2014.03.050