N₂-((1E)-2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-ylidene)-N₁,N₁-dimethyl-1,2-ethanediamine

Base Information

• Chemical Name: N₂-((1E)-2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-ylidene)-N₁,N₁-dimethyl-1,2-ethanediamine
• CAS No.: 1210405-89-2
• Molecular Formula: C₂₂H₃₅N₃
• Molecular Weight: 341.54

Synonyms:N₂-((1E)-2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-ylidene)-N₁,N₁-dimethyl-1,2-ethanediamine

Chemical Property of N₂-((1E)-2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-ylidene)-N₁,N₁-dimethyl-1,2-ethanediamine

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Technology Process of N₂-((1E)-2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-ylidene)-N₁,N₁-dimethyl-1,2-ethanediamine

There total 3 articles about N₂-((1E)-2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-ylidene)-N₁,N₁-dimethyl-1,2-ethanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.97%

2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-one (1210405-73-4) + N,N-dimethylethylenediamine (108-00-9) → N2-((1E)-2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-ylidene)-N1,N1-dimethyl-1,2-ethanediamine (1210405-89-2)

Guidance literature:

N,N-dimethylethylenediamine; With titanium tetrachloride; In toluene; for 1h;

2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-one; In toluene; for 3h;

Reference yield:

2-morpholinocyclohex-2-enone (23740-64-9) → N2-((1E)-2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-ylidene)-N1,N1-dimethyl-1,2-ethanediamine (1210405-89-2)

Guidance literature:

Multi-step reaction with 2 steps

1: p-toluenesulfonic acid monohydrate / toluene

2: titanium tetrachloride / toluene

With p-toluenesulfonic acid monohydrate; titanium tetrachloride; In toluene;

Reference yield:

2,6-diisopropylbenzenamine (24544-04-5) → N2-((1E)-2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-ylidene)-N1,N1-dimethyl-1,2-ethanediamine (1210405-89-2)

Guidance literature:

Multi-step reaction with 2 steps

1: p-toluenesulfonic acid monohydrate / toluene

2: titanium tetrachloride / toluene

With p-toluenesulfonic acid monohydrate; titanium tetrachloride; In toluene;

upstream raw materials:

2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-one

N,N-dimethylethylenediamine

2,6-diisopropylbenzenamine

2-morpholinocyclohex-2-enone

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