ethyl 5,6-diamino-4--2-pyridinecarbamate hydrochloride

Base Information

Chemical Name:ethyl 5,6-diamino-4--2-pyridinecarbamate hydrochloride
CAS No.:83269-24-3
Molecular Formula:25C₁₇H₂₃N₅O₃*62ClH
Molecular Weight:10895.6
Hs Code.:

ethyl 5,6-diamino-4-<N-(2-hydroxy-2-phenylethyl)-N-methylamino>-2-pyridinecarbamate hydrochloride

Synonyms:ethyl 5,6-diamino-4--2-pyridinecarbamate hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 5,6-diamino-4--2-pyridinecarbamate hydrochloride

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Technology Process of ethyl 5,6-diamino-4--2-pyridinecarbamate hydrochloride

There total 3 articles about ethyl 5,6-diamino-4--2-pyridinecarbamate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 83269-22-1
ethyl 6-amino-4--5-nitro-2-pyridinecarbamate

: 83269-24-3
ethyl 5,6-diamino-4--2-pyridinecarbamate hydrochloride

Guidance literature:: With hydrogen; nickel; In ethanol; for 1h; under 760 Torr; Ambient temperature;
DOI:10.1021/jm00355a018

Reference yield:

: 68579-60-2,6589-55-5
2-(methylamino)-1-phenylethanol

: 83269-24-3
ethyl 5,6-diamino-4--2-pyridinecarbamate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / ethanol / 2 h / Heating

2: 85 percent / H₂ / Raney nickel / ethanol / 1 h / 760 Torr / Ambient temperature

With hydrogen; triethylamine; nickel; In ethanol;
DOI:10.1021/jm00355a018

Reference yield:

: 6506-86-1
ethyl (6-amino-4-chloro-5-nitropyridin-2-yl)carbamate

: 83269-24-3
ethyl 5,6-diamino-4--2-pyridinecarbamate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / ethanol / 2 h / Heating

2: 85 percent / H₂ / Raney nickel / ethanol / 1 h / 760 Torr / Ambient temperature

With hydrogen; triethylamine; nickel; In ethanol;
DOI:10.1021/jm00355a018