Benzyl 2,4-bis(benzyloxy)-3,5,6-trifluorobenzoate

Base Information

Chemical Name:Benzyl 2,4-bis(benzyloxy)-3,5,6-trifluorobenzoate
CAS No.:197903-55-2
Molecular Formula:C₂₈H₂₁F₃O₄
Molecular Weight:478.468
Hs Code.:

Synonyms:Benzyl 2,4-bis(benzyloxy)-3,5,6-trifluorobenzoate

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Chemical Property of Benzyl 2,4-bis(benzyloxy)-3,5,6-trifluorobenzoate

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Technology Process of Benzyl 2,4-bis(benzyloxy)-3,5,6-trifluorobenzoate

There total 5 articles about Benzyl 2,4-bis(benzyloxy)-3,5,6-trifluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 197903-54-1
Benzyl 4-benzyloxy-2,3,5,6-tetrafluorobenzoate

: 100-51-6,185532-71-2
benzyl alcohol

: 197903-55-2
Benzyl 2,4-bis(benzyloxy)-3,5,6-trifluorobenzoate

: Benzyl 2,4,6-tris(benzyloxy)-3,5-difluorobenzoate

Guidance literature:: benzyl alcohol; With potassium tert-butylate; In tetrahydrofuran; for 0.5h;

Benzyl 4-benzyloxy-2,3,5,6-tetrafluorobenzoate; In tetrahydrofuran; at 20 ℃; for 1.5h;
DOI:10.1039/b007101n

Reference yield: 62.0%

: 100-51-6,185532-71-2
benzyl alcohol

: 104856-46-4
benzyl 2,3,4,5,6-pentafluorobenzoate

: 197903-55-2
Benzyl 2,4-bis(benzyloxy)-3,5,6-trifluorobenzoate

: Benzyl 2,4,6-tris(benzyloxy)-3,5-difluorobenzoate

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)02252-8

Reference yield:

: 100-39-0
benzyl bromide

: 197903-55-2
Benzyl 2,4-bis(benzyloxy)-3,5,6-trifluorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: CsCO₃ / dimethylformamide

2: 62 percent / KOtBu / tetrahydrofuran

With potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)02252-8