ethyl 4-hydroxy-5-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3-carboxylate

Base Information

Chemical Name:ethyl 4-hydroxy-5-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3-carboxylate
CAS No.:1616404-15-9
Molecular Formula:C₁₄H₁₂ClNO₄
Molecular Weight:293.707
Hs Code.:

Synonyms:ethyl 4-hydroxy-5-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3-carboxylate

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Chemical Property of ethyl 4-hydroxy-5-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3-carboxylate

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Technology Process of ethyl 4-hydroxy-5-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3-carboxylate

There total 4 articles about ethyl 4-hydroxy-5-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1616404-09-1
C₁₆H₁₈ClNO₅

: 1616404-15-9
ethyl 4-hydroxy-5-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3-carboxylate

Guidance literature:: In 5,5-dimethyl-1,3-cyclohexadiene; for 12h; Reflux;
DOI:10.1080/00397911.2013.878360

Reference yield:

: 132606-72-5
4-chlorocinnamyl isocyanate

: 1616404-15-9
ethyl 4-hydroxy-5-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / toluene; mineral oil

1.2: 2 h / 0 - 20 °C

2.1: 5,5-dimethyl-1,3-cyclohexadiene / 12 h / Reflux

With sodium hydride; In 5,5-dimethyl-1,3-cyclohexadiene; toluene; mineral oil;
DOI:10.1080/00397911.2013.878360

Reference yield:

: 83421-78-7
(E)-3-(4-Chloro-phenyl)-acryloyl azide

: 1616404-15-9
ethyl 4-hydroxy-5-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzine / Reflux

2.1: sodium hydride / toluene; mineral oil

2.2: 2 h / 0 - 20 °C

3.1: 5,5-dimethyl-1,3-cyclohexadiene / 12 h / Reflux

With sodium hydride; In benzine; 5,5-dimethyl-1,3-cyclohexadiene; toluene; mineral oil; 1.1: |Curtius Rearrangement;
DOI:10.1080/00397911.2013.878360