methyl (2S,4R)-4-[(tert-butoxycarbonyl)(p-toluenesulfonyl)amino]-2-methyl-5-phenylpentanoate

Base Information

Chemical Name:methyl (2S,4R)-4-[(tert-butoxycarbonyl)(p-toluenesulfonyl)amino]-2-methyl-5-phenylpentanoate
CAS No.:919518-36-8
Molecular Formula:C₂₅H₃₃NO₆S
Molecular Weight:475.606
Hs Code.:

Synonyms:methyl (2S,4R)-4-[(tert-butoxycarbonyl)(p-toluenesulfonyl)amino]-2-methyl-5-phenylpentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2S,4R)-4-[(tert-butoxycarbonyl)(p-toluenesulfonyl)amino]-2-methyl-5-phenylpentanoate

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Technology Process of methyl (2S,4R)-4-[(tert-butoxycarbonyl)(p-toluenesulfonyl)amino]-2-methyl-5-phenylpentanoate

There total 2 articles about methyl (2S,4R)-4-[(tert-butoxycarbonyl)(p-toluenesulfonyl)amino]-2-methyl-5-phenylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 362495-90-7
[2S,4R]-(-)-2-methyl-5-phenyl-4-(p-toluenesulfonylamino)pentanoic acid

: 919518-36-8
methyl (2S,4R)-4-[(tert-butoxycarbonyl)(p-toluenesulfonyl)amino]-2-methyl-5-phenylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / HCl / 16 h / Heating

2: 93 percent / DMAP / acetonitrile / 20 °C

With hydrogenchloride; dmap; In acetonitrile;
DOI:10.1002/anie.200601259

Reference yield:

: 362495-79-2
[2S,4R,1'S,2'S]-(+)-N,2-dimethyl-5-phenyl-N-(2'-phenyl-2'-hydroxy-1'-methylethyl)-4-(p-toluenesulfonylamino)pentanamide

: 919518-36-8
methyl (2S,4R)-4-[(tert-butoxycarbonyl)(p-toluenesulfonyl)amino]-2-methyl-5-phenylpentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: H₂SO₄ / dioxane / 5 h / Heating

2: 85 percent / HCl / 16 h / Heating

3: 93 percent / DMAP / acetonitrile / 20 °C

With hydrogenchloride; dmap; sulfuric acid; In 1,4-dioxane; acetonitrile;
DOI:10.1002/anie.200601259