3-benzenesulfonyl-4-((6-((2-methoxyethoxy)methoxy)-2,5,7,8-tetramethylchroman-2-yl)methoxy)furoxan

Base Information

Chemical Name:3-benzenesulfonyl-4-((6-((2-methoxyethoxy)methoxy)-2,5,7,8-tetramethylchroman-2-yl)methoxy)furoxan
CAS No.:893403-91-3
Molecular Formula:C₂₆H₃₂N₂O₉S
Molecular Weight:548.614
Hs Code.:

Synonyms:3-benzenesulfonyl-4-((6-((2-methoxyethoxy)methoxy)-2,5,7,8-tetramethylchroman-2-yl)methoxy)furoxan

Suppliers and Price of 3-benzenesulfonyl-4-((6-((2-methoxyethoxy)methoxy)-2,5,7,8-tetramethylchroman-2-yl)methoxy)furoxan

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-benzenesulfonyl-4-((6-((2-methoxyethoxy)methoxy)-2,5,7,8-tetramethylchroman-2-yl)methoxy)furoxan

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-benzenesulfonyl-4-((6-((2-methoxyethoxy)methoxy)-2,5,7,8-tetramethylchroman-2-yl)methoxy)furoxan

There total 3 articles about 3-benzenesulfonyl-4-((6-((2-methoxyethoxy)methoxy)-2,5,7,8-tetramethylchroman-2-yl)methoxy)furoxan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 820976-58-7
[6-(methoxyethoxymethoxy)-2,5,7,8-tetramethyl-3,4-dihydro-2H-chroman-2-yl]methanol

: 66074-00-8
3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide

: 893403-91-3
3-benzenesulfonyl-4-((6-((2-methoxyethoxy)methoxy)-2,5,7,8-tetramethylchroman-2-yl)methoxy)furoxan

Guidance literature:: [6-(methoxyethoxymethoxy)-2,5,7,8-tetramethyl-3,4-dihydro-2H-chroman-2-yl]methanol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide; In tetrahydrofuran; at 30 ℃;
DOI:10.1021/jm0510530

Reference yield:

: 820976-57-6
ethyl 6-((2-methoxyethoxy)methoxy)-2,5,7,8-tetramethylchromane-2-carboxylate

: 893403-91-3
3-benzenesulfonyl-4-((6-((2-methoxyethoxy)methoxy)-2,5,7,8-tetramethylchroman-2-yl)methoxy)furoxan

Guidance literature:: Multi-step reaction with 2 steps

1.1: 84 percent / LiAlH₄ / tetrahydrofuran / 1.5 h / 20 °C

2.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

2.2: 60 percent / tetrahydrofuran / 30 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jm0510530

Reference yield:

: 53174-07-5
ethyl 6-hydroxy-2,5,7,8-tetramethyl-3,4-dihydro-2H-chromene-2-carboxylate

: 893403-91-3
3-benzenesulfonyl-4-((6-((2-methoxyethoxy)methoxy)-2,5,7,8-tetramethylchroman-2-yl)methoxy)furoxan

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran / 20 °C

1.2: 74 percent / tetrahydrofuran / 25 h

2.1: 84 percent / LiAlH₄ / tetrahydrofuran / 1.5 h / 20 °C

3.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

3.2: 60 percent / tetrahydrofuran / 30 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jm0510530