S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-acetyl sulfoximide

Base Information

Chemical Name:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-acetyl sulfoximide
CAS No.:1147095-63-3
Molecular Formula:C₂₂H₁₈Cl₂N₄O₄S
Molecular Weight:505.381
Hs Code.:

Synonyms:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-acetyl sulfoximide

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Chemical Property of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-acetyl sulfoximide

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Technology Process of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-acetyl sulfoximide

There total 13 articles about S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-acetyl sulfoximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1147095-59-7,1147096-64-7
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl sulfoximide

: 75-36-5
acetyl chloride

: 1147095-63-3
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-acetyl sulfoximide

Guidance literature:: With pyridine; In dichloromethane; at 10 - 30 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.ejmech.2012.10.005

Reference yield: 61.0%

: 1147095-63-3
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-acetyl sulfoximide

Guidance literature:

Reference yield:

: 114129-35-0
methyl 4-(methylsulfinyl)benzoate

: 1147095-63-3
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-acetyl sulfoximide

Guidance literature:: Multi-step reaction with 7 steps

1: sodium azide; sulfuric acid / chloroform / 15 h / -20 - 50 °C / Inert atmosphere

2: pyridine / dichloromethane; toluene / 3 h / 15 - 30 °C / Inert atmosphere

3: water; sodium hydroxide / tetrahydrofuran / 3 h / 25 - 30 °C

4: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

5: tetrahydrofuran / 2 h / 10 - 30 °C / Inert atmosphere

6: sulfuric acid / 0 - 5 °C

7: pyridine / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

With pyridine; sodium azide; oxalyl dichloride; sulfuric acid; water; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; dichloromethane; chloroform; toluene;
DOI:10.1016/j.ejmech.2012.10.005