Technology Process of C33H31O5P
There total 8 articles about C33H31O5P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
dichloromethane;
at 15 - 30 ℃;
- Guidance literature:
-
With
potassium carbonate;
In
acetonitrile;
at 30 - 45 ℃;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium cyanide / water / 30 - 45 °C
2: sulfuric acid / 20 °C
3: 1H-imidazole / dichloromethane; ethyl acetate / 25 - 30 °C
4: N-iodo-succinimide / acetone / 0 - 25 °C
5: sodium hydrogencarbonate; sodium hypochlorite; tetrabutylammomium bromide; dihydrogen peroxide; potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / -10 - 20 °C
6: potassium carbonate / acetonitrile / 30 - 45 °C
With
1H-imidazole; sodium cyanide; sodium hypochlorite; N-iodo-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sulfuric acid; tetrabutylammomium bromide; dihydrogen peroxide; sodium hydrogencarbonate; potassium carbonate; potassium bromide;
In
dichloromethane; water; ethyl acetate; acetone; acetonitrile;
6: Wittig Reaction;