trichloroethyl 2β-(chloromethyl)-2α-methyl-6β-(N-nitrosophenoxyacetamido)-penam-3α-carboxylate

Base Information

Chemical Name:trichloroethyl 2β-(chloromethyl)-2α-methyl-6β-(N-nitrosophenoxyacetamido)-penam-3α-carboxylate
CAS No.:138976-41-7
Molecular Formula:C₁₈H₁₇Cl₄N₃O₆S
Molecular Weight:545.227
Hs Code.:

Synonyms:trichloroethyl 2β-(chloromethyl)-2α-methyl-6β-(N-nitrosophenoxyacetamido)-penam-3α-carboxylate

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Chemical Property of trichloroethyl 2β-(chloromethyl)-2α-methyl-6β-(N-nitrosophenoxyacetamido)-penam-3α-carboxylate

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Technology Process of trichloroethyl 2β-(chloromethyl)-2α-methyl-6β-(N-nitrosophenoxyacetamido)-penam-3α-carboxylate

There total 1 articles about trichloroethyl 2β-(chloromethyl)-2α-methyl-6β-(N-nitrosophenoxyacetamido)-penam-3α-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.4%

: 51415-42-0
trichloroethyl 2β-(chloromethyl)-2α-methyl-6β-(phenoxyacetamido)-penam-3α-carboxylate

: 138976-41-7
trichloroethyl 2β-(chloromethyl)-2α-methyl-6β-(N-nitrosophenoxyacetamido)-penam-3α-carboxylate

Guidance literature:: With sodium acetate; dinitrogen tetraoxide; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/0223-5234(91)90005-8

Reference yield: 98.7%

: 138976-41-7
trichloroethyl 2β-(chloromethyl)-2α-methyl-6β-(N-nitrosophenoxyacetamido)-penam-3α-carboxylate

: 138976-42-8
trichloroethyl 2β-(chloromethyl)-2α-methyl-6β-(N-nitrosophenoxyacetamido)-penam-3α-carboxylate 1R-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/0223-5234(91)90005-8

Reference yield:

: 138976-41-7
trichloroethyl 2β-(chloromethyl)-2α-methyl-6β-(N-nitrosophenoxyacetamido)-penam-3α-carboxylate

: 104641-33-0
trichloroethyl 2α-(chloromethyl)-2β-methyl-6β-(phenoxyacetamido)-penam-3α-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 98.7 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 0 °C

2: 90 percent / H₂ / 10percent Pd/C / ethyl acetate / 1.5 h / 310.4 Torr

3: 46.7 percent / toluene / 0.33 h / Heating

4: 30.3 percent / PBr₃ / dimethylformamide / 1.75 h / 0 °C

With hydrogen; phosphorus tribromide; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1016/0223-5234(91)90005-8