5-acetamido-3,4-di-O-benzyl-5-deoxy-1,2-O-isopropylidene-L-talo-quercitol

Base Information

Chemical Name:5-acetamido-3,4-di-O-benzyl-5-deoxy-1,2-O-isopropylidene-L-talo-quercitol
CAS No.:861661-18-9
Molecular Formula:C₂₅H₃₁NO₅
Molecular Weight:425.525
Hs Code.:

Synonyms:5-acetamido-3,4-di-O-benzyl-5-deoxy-1,2-O-isopropylidene-L-talo-quercitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-acetamido-3,4-di-O-benzyl-5-deoxy-1,2-O-isopropylidene-L-talo-quercitol

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Technology Process of 5-acetamido-3,4-di-O-benzyl-5-deoxy-1,2-O-isopropylidene-L-talo-quercitol

There total 1 articles about 5-acetamido-3,4-di-O-benzyl-5-deoxy-1,2-O-isopropylidene-L-talo-quercitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 5-acetamido-5-deoxy-1,2-O-isopropylidenequercitol

: 100-39-0
benzyl bromide

: 861661-18-9
5-acetamido-3,4-di-O-benzyl-5-deoxy-1,2-O-isopropylidene-L-talo-quercitol

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 72h;
DOI:10.1016/j.bmc.2005.04.003

Reference yield:

: 861661-18-9
5-acetamido-3,4-di-O-benzyl-5-deoxy-1,2-O-isopropylidene-L-talo-quercitol

: 72075-06-0
(1R,2R,3S,4R,5R)-5-aminocyclohexa-1,2,3,4-tetraol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 100 percent / acetic acid / H₂O / 1.5 h / 50 °C

2.1: H₂; hydrochloric acid / Pd/C / ethanol / 14 h / 20 °C / atmospheric pressure

2.2: 100 percent / hydrochloric acid / 15 h / 80 °C

With hydrogenchloride; hydrogen; acetic acid; palladium on activated charcoal; In ethanol; water;
DOI:10.1016/j.bmc.2005.04.003