3,3'-dinitrodiphenyl sulfide

Base Information

Chemical Name:3,3'-dinitrodiphenyl sulfide
CAS No.:37755-03-6
Molecular Formula:C₁₂H₈N₂O₄S
Molecular Weight:276.273
Hs Code.:

Synonyms:3,3'-dinitrodiphenyl sulfide

Suppliers and Price of 3,3'-dinitrodiphenyl sulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3'-dinitrodiphenyl sulfide

Chemical Property:

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Technology Process of 3,3'-dinitrodiphenyl sulfide

There total 9 articles about 3,3'-dinitrodiphenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 645-00-1
m-iodonitrobenzene

: 37755-03-6
3,3'-dinitrodiphenyl sulfide

Guidance literature:: With potassium thioacyanate; cetyltrimethylammonim bromide; potassium hydroxide; In water; at 135 ℃; for 7h; Green chemistry;
DOI:10.1002/aoc.3471

Reference yield: 88.0%

: 645-00-1
m-iodonitrobenzene

: 3814-18-4
3-nitrothiophenol

: 37755-03-6
3,3'-dinitrodiphenyl sulfide

Guidance literature:: With triethylamine; In neat (no solvent); at 90 ℃; for 7h; chemoselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201300416

Reference yield: 85.0%

: 645-00-1
m-iodonitrobenzene

: 62-55-5
thioacetamide

: 37755-03-6
3,3'-dinitrodiphenyl sulfide

Guidance literature:: With caesium carbonate; In water; dimethyl sulfoxide; at 120 ℃; for 24h; Schlenk technique; Inert atmosphere; Sealed tube; Green chemistry;
DOI:10.1016/j.molcata.2014.08.010