dicarbonyldibromobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

Base Information

Chemical Name:dicarbonyldibromobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)
CAS No.:80462-15-3
Molecular Formula:C₄₄H₃₆Br₂Ir₂N₄O₂P₂
Molecular Weight:1258.99
Hs Code.:

Synonyms:dicarbonyldibromobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

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Chemical Property of dicarbonyldibromobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

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Technology Process of dicarbonyldibromobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

There total 3 articles about dicarbonyldibromobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 98420-38-3
dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)

: 80462-15-3
dicarbonyldibromobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

Guidance literature:: With Br₂; In tetrahydrofuran; diethyl ether; under N2, Ir-complex in Et2O-THF was treated with 1 equiv of Br2 in Et2O; solid collected, washed with hexane, dried; elem. anal.;

Reference yield:

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 80462-15-3
dicarbonyldibromobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: Br₂ / tetrahydrofuran; diethyl ether

With Br₂; In tetrahydrofuran; diethyl ether;

Reference yield:

: 101010-16-6
{Ir2(μ-η2-pyrazolate)2(η4-1,4-cyclooctadiene)2}

: 80462-15-3
dicarbonyldibromobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

Guidance literature:: Multi-step reaction with 2 steps

1: CO; triphenylphosphine / tetrahydrofuran

2: Br₂ / tetrahydrofuran; diethyl ether

With CO; triphenylphosphine; Br₂; In tetrahydrofuran; diethyl ether;