dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)

Base Information

Chemical Name:dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)
CAS No.:98420-38-3
Molecular Formula:C₄₄H₃₆Ir₂N₄O₂P₂
Molecular Weight:1099.18
Hs Code.:

Synonyms:dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)

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Chemical Property of dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)

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Technology Process of dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)

There total 4 articles about dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 288-13-1
NH-pyrazole

: chloro(1,5-cyclooctadiene)iridium(I) dimer

: 98420-38-3
dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)

Guidance literature:: With CO; PPh₃; In triethylamine; ((COD)IrCl)2 treated with pyrazole/triethylamine; COD displaced with CO;react. with PPh3;
DOI:10.1021/ja00367a075

Reference yield:

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 98420-38-3
dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)

Guidance literature:: In tetrahydrofuran; reaction of Ir-complex with pyrazolides at 6 h at ambient temp.;
DOI:10.1021/ja00367a075

Reference yield:

: 101010-16-6
{Ir2(μ-η2-pyrazolate)2(η4-1,4-cyclooctadiene)2}

: 98420-38-3
dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)

: 92283-13-1
(Ir(CO)(P(C₆H₅)3)(C₃H₃N₂))2*C₆H₁₄

Guidance literature:: With CO; triphenylphosphine; In tetrahydrofuran; under N2, CO was bubbled through soln. of Ir-complex in THF, solvent removed, PPh3 in hexane was added, 15 min; concd., hexane added as upper layer;