1,3,5-tri-tert-butyl ((benzenetricarbonyltris(azanediyl)) tris(ethane-2,1-diyl))tricarbamate

Base Information

Chemical Name:1,3,5-tri-tert-butyl ((benzenetricarbonyltris(azanediyl)) tris(ethane-2,1-diyl))tricarbamate
CAS No.:862299-07-8
Molecular Formula:C₃₀H₄₈N₆O₉
Molecular Weight:636.746
Hs Code.:

Synonyms:1,3,5-tri-tert-butyl ((benzenetricarbonyltris(azanediyl)) tris(ethane-2,1-diyl))tricarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,5-tri-tert-butyl ((benzenetricarbonyltris(azanediyl)) tris(ethane-2,1-diyl))tricarbamate

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Technology Process of 1,3,5-tri-tert-butyl ((benzenetricarbonyltris(azanediyl)) tris(ethane-2,1-diyl))tricarbamate

There total 4 articles about 1,3,5-tri-tert-butyl ((benzenetricarbonyltris(azanediyl)) tris(ethane-2,1-diyl))tricarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 57260-73-8
N-BOC-1,2-diaminoethane

: 4422-95-1
1,3,5-benzene tris(carbonyl chloride)

: 862299-07-8
1,3,5-tri-tert-butyl ((benzenetricarbonyltris(azanediyl)) tris(ethane-2,1-diyl))tricarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 2h; Inert atmosphere;
DOI:10.1021/acs.molpharmaceut.5b00358

Reference yield:

: C₄₈H₇₂N₆O₆

: 57260-73-8
N-BOC-1,2-diaminoethane

: 862299-07-8
1,3,5-tri-tert-butyl ((benzenetricarbonyltris(azanediyl)) tris(ethane-2,1-diyl))tricarbamate

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1021/ja060720r

Reference yield:

: 57260-73-8
N-BOC-1,2-diaminoethane

: 554-95-0
benzene-1,3,5-tricarboxylic acid

: 862299-07-8
1,3,5-tri-tert-butyl ((benzenetricarbonyltris(azanediyl)) tris(ethane-2,1-diyl))tricarbamate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo0709293