(S)-tert-butyl 2-((S)-2-(hydroxyamino)propanamido)-3-phenylpropanoate oxalate

Base Information

• Chemical Name: (S)-tert-butyl 2-((S)-2-(hydroxyamino)propanamido)-3-phenylpropanoate oxalate
• CAS No.: 1243692-08-1
• Molecular Formula: C₂H₂O₄*C₁₆H₂₄N₂O₄
• Molecular Weight: 398.413

Synonyms:(S)-tert-butyl 2-((S)-2-(hydroxyamino)propanamido)-3-phenylpropanoate oxalate

Chemical Property of (S)-tert-butyl 2-((S)-2-(hydroxyamino)propanamido)-3-phenylpropanoate oxalate

Chemical Property:

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Technology Process of (S)-tert-butyl 2-((S)-2-(hydroxyamino)propanamido)-3-phenylpropanoate oxalate

There total 1 articles about (S)-tert-butyl 2-((S)-2-(hydroxyamino)propanamido)-3-phenylpropanoate oxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

(S)-N-benzylidene-1-((S)-1-tert-butoxy-1-oxo-3-phenylpropan-2-ylamino)-1-oxopropan-2-amine oxide (1243692-38-7) + oxalic acid (144-62-7,97993-78-7) → (S)-tert-butyl 2-((S)-2-(hydroxyamino)propanamido)-3-phenylpropanoate oxalate (1243692-08-1)

Guidance literature:

(S)-N-benzylidene-1-((S)-1-tert-butoxy-1-oxo-3-phenylpropan-2-ylamino)-1-oxopropan-2-amine oxide; With hydroxylamine hydrochloride; In methanol; at 40 ℃;

oxalic acid; In methanol;

DOI:10.1039/c004490c

Reference yield: 50.0%

(S)-3-((S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)propanamido)-2-oxo-4-phenylbutanoic acid (1019690-85-7) + (S)-tert-butyl 2-((S)-2-(hydroxyamino)propanamido)-3-phenylpropanoate oxalate (1243692-08-1) → (5S,8S,11S,14S)-tert-butyl 8,14-dibenzyl-1-(9H-fluoren-9-yl)-5,11-dimethyl-3,6,9,12-tetraoxo-2-oxa-4,7,10,13-tetraazapentadecan-15-oate (1243692-11-6)

Guidance literature:

In N,N-dimethyl-formamide; at 40 ℃;

DOI:10.1039/c004490c

upstream raw materials:

(S)-N-benzylidene-1-((S)-1-tert-butoxy-1-oxo-3-phenylpropan-2-ylamino)-1-oxopropan-2-amine oxide

oxalic acid

Downstream raw materials:

(5S,8S,11S,14S)-tert-butyl 8,14-dibenzyl-1-(9H-fluoren-9-yl)-5,11-dimethyl-3,6,9,12-tetraoxo-2-oxa-4,7,10,13-tetraazapentadecan-15-oate

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