C₁₃H₁₂O₃

Base Information

Chemical Name:C₁₃H₁₂O₃
CAS No.:1393726-88-9
Molecular Formula:C₁₃H₁₂O₃
Molecular Weight:216.236
Hs Code.:

C<sub>13</sub>H<sub>12</sub>O<sub>3</sub>

Synonyms:C₁₃H₁₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₂O₃

Chemical Property:

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Technology Process of C₁₃H₁₂O₃

There total 3 articles about C₁₃H₁₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1393726-85-6
C₁₈H₂₀O₄

: 1393726-88-9
C₁₃H₁₂O₃

Guidance literature:: With pyridinium p-toluenesulfonate; In ethanol; at 20 ℃; for 6h;
DOI:10.1016/j.tet.2012.06.001

Reference yield:

: 253435-18-6
2-(3-(2-tetrahydropyranyloxy)-1-propynyl)-1-iodobenzene

: 1393726-88-9
C₁₃H₁₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 4 h / 110 °C

2: pyridinium p-toluenesulfonate / ethanol / 6 h / 20 °C

With tetrabutylammomium bromide; palladium diacetate; pyridinium p-toluenesulfonate; potassium carbonate; triphenylphosphine; In ethanol; N,N-dimethyl-formamide; 1: Heck coupling;
DOI:10.1016/j.tet.2012.06.001

Reference yield:

: 615-42-9
1,2-Diiodobenzene

: 1393726-88-9
C₁₃H₁₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 2.5 h / 20 °C

2: tetrabutylammomium bromide; palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 4 h / 110 °C

3: pyridinium p-toluenesulfonate / ethanol / 6 h / 20 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; palladium diacetate; pyridinium p-toluenesulfonate; potassium carbonate; triethylamine; triphenylphosphine; In ethanol; N,N-dimethyl-formamide; 1: Sonogashira coupling / 2: Heck coupling;
DOI:10.1016/j.tet.2012.06.001