Technology Process of C40H56N4O5Si
There total 11 articles about C40H56N4O5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate; sodium iodide;
In
dimethyl sulfoxide;
at 140 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium hydroxide / tetrabutylammomium bromide / water / 5 h / 20 °C
2: cetyltributylphosphonium bromide / N,N-dimethyl-formamide / 3 h / 75 °C
3: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C / 2070.21 Torr
4: triethylamine / dichloromethane / 20 °C
5: N-ethyl-N,N-diisopropylamine / 120 °C
6: hydrazine / ethanol / 22 h / 20 °C
7: sodium hydrogencarbonate; sodium iodide / dimethyl sulfoxide / 2 h / 140 °C
With
sodium hydroxide; hydrogen; sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; hydrazine;
palladium 10% on activated carbon; tetrabutylammomium bromide; cetyltributylphosphonium bromide;
In
methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: cetyltributylphosphonium bromide / N,N-dimethyl-formamide / 3 h / 75 °C
2: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C / 2070.21 Torr
3: triethylamine / dichloromethane / 20 °C
4: N-ethyl-N,N-diisopropylamine / 120 °C
5: hydrazine / ethanol / 22 h / 20 °C
6: sodium hydrogencarbonate; sodium iodide / dimethyl sulfoxide / 2 h / 140 °C
With
hydrogen; sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; hydrazine;
palladium 10% on activated carbon; cetyltributylphosphonium bromide;
In
methanol; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;