(Z)-3-(1-carboxy-2-phenylethyl)-5-(4-trifluoromethylbenzylidene)hydantoin

Base Information

Chemical Name:(Z)-3-(1-carboxy-2-phenylethyl)-5-(4-trifluoromethylbenzylidene)hydantoin
CAS No.:133384-48-2
Molecular Formula:C₂₀H₁₅F₃N₂O₄
Molecular Weight:404.345
Hs Code.:

Synonyms:(Z)-3-(1-carboxy-2-phenylethyl)-5-(4-trifluoromethylbenzylidene)hydantoin

Suppliers and Price of (Z)-3-(1-carboxy-2-phenylethyl)-5-(4-trifluoromethylbenzylidene)hydantoin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-(1-carboxy-2-phenylethyl)-5-(4-trifluoromethylbenzylidene)hydantoin

Chemical Property:

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Technology Process of (Z)-3-(1-carboxy-2-phenylethyl)-5-(4-trifluoromethylbenzylidene)hydantoin

There total 3 articles about (Z)-3-(1-carboxy-2-phenylethyl)-5-(4-trifluoromethylbenzylidene)hydantoin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 133384-48-2
(Z)-3-(1-carboxy-2-phenylethyl)-5-(4-trifluoromethylbenzylidene)hydantoin

Guidance literature:: Multi-step reaction with 2 steps

1: 31 percent / trimethylamine (25-30percent in water) / H₂O; methanol / 1) 22h, reflux, 2) 24h, r.t.

2: 100 percent / HBr (48percent in water) / 47 h / Heating

With hydrogen bromide; trimethylamine; In methanol; water;
DOI:10.1039/P19900003129

Reference yield:

: 70288-60-7,73136-26-2,124916-61-6,3196-22-3
methyl 2-bromo-3-phenylpropionate

: 133384-48-2
(Z)-3-(1-carboxy-2-phenylethyl)-5-(4-trifluoromethylbenzylidene)hydantoin

Guidance literature:: Multi-step reaction with 3 steps

1: 1) sodium methoxide / 1) methanol, reflux, overnight, 2) 10 d, 50 deg C

2: 31 percent / trimethylamine (25-30percent in water) / H₂O; methanol / 1) 22h, reflux, 2) 24h, r.t.

3: 100 percent / HBr (48percent in water) / 47 h / Heating

With hydrogen bromide; sodium methylate; trimethylamine; In methanol; water;
DOI:10.1039/P19900003129

Reference yield:

: 133384-44-8
3-(1-methoxycarbonyl-2-phenylethyl)hydantoin

: 133384-48-2
(Z)-3-(1-carboxy-2-phenylethyl)-5-(4-trifluoromethylbenzylidene)hydantoin

Guidance literature:: Multi-step reaction with 2 steps

1: 31 percent / trimethylamine (25-30percent in water) / H₂O; methanol / 1) 22h, reflux, 2) 24h, r.t.

2: 100 percent / HBr (48percent in water) / 47 h / Heating

With hydrogen bromide; trimethylamine; In methanol; water;
DOI:10.1039/P19900003129