8-iodomethyl-1-phenyl-6-(prop-2-en-1-yl)-7,8-dihydro-1H-imidazo[1,2-a]-pyrazolo[4,3-e]pyrimidin-4(6H)-one

Base Information

• Chemical Name: 8-iodomethyl-1-phenyl-6-(prop-2-en-1-yl)-7,8-dihydro-1H-imidazo[1,2-a]-pyrazolo[4,3-e]pyrimidin-4(6H)-one
• CAS No.: 1331826-52-8
• Molecular Formula: C₁₇H₁₆IN₅O
• Molecular Weight: 433.251

Synonyms:8-iodomethyl-1-phenyl-6-(prop-2-en-1-yl)-7,8-dihydro-1H-imidazo[1,2-a]-pyrazolo[4,3-e]pyrimidin-4(6H)-one

Chemical Property of 8-iodomethyl-1-phenyl-6-(prop-2-en-1-yl)-7,8-dihydro-1H-imidazo[1,2-a]-pyrazolo[4,3-e]pyrimidin-4(6H)-one

Chemical Property:

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Technology Process of 8-iodomethyl-1-phenyl-6-(prop-2-en-1-yl)-7,8-dihydro-1H-imidazo[1,2-a]-pyrazolo[4,3-e]pyrimidin-4(6H)-one

There total 3 articles about 8-iodomethyl-1-phenyl-6-(prop-2-en-1-yl)-7,8-dihydro-1H-imidazo[1,2-a]-pyrazolo[4,3-e]pyrimidin-4(6H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

6-bis(prop-2-en-1-yl)amino-1-phenyl-1H-pyrazolo[3,4-d]-pyrimidin-4(5H)-one (1219026-96-6) → 8-iodomethyl-1-phenyl-6-(prop-2-en-1-yl)-7,8-dihydro-1H-imidazo[1,2-a]-pyrazolo[4,3-e]pyrimidin-4(6H)-one (1331826-52-8)

Guidance literature:

6-bis(prop-2-en-1-yl)amino-1-phenyl-1H-pyrazolo[3,4-d]-pyrimidin-4(5H)-one; With iodine; acetic acid; at 20 ℃; for 24h;

With sodium sulfite; In acetonitrile; at 20 ℃;

DOI:10.1134/S1070428011070165

Reference yield:

6-chloro-1-phenyl-1,5-dihydro-4H-pyrazolo[3,4-d]pyrimidin-4-one (6288-99-9) → 8-iodomethyl-1-phenyl-6-(prop-2-en-1-yl)-7,8-dihydro-1H-imidazo[1,2-a]-pyrazolo[4,3-e]pyrimidin-4(6H)-one (1331826-52-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ethanol / 4 h / 90 - 100 °C / Sealed ampule

2.1: iodine; acetic acid / 24 h / 20 °C

2.2: 20 °C

With iodine; acetic acid; In ethanol;

DOI:10.1134/S1070428011070165

Reference yield:

diallylamine (124-02-7) → 8-iodomethyl-1-phenyl-6-(prop-2-en-1-yl)-7,8-dihydro-1H-imidazo[1,2-a]-pyrazolo[4,3-e]pyrimidin-4(6H)-one (1331826-52-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ethanol / 4 h / 90 - 100 °C / Sealed ampule

2.1: iodine; acetic acid / 24 h / 20 °C

2.2: 20 °C

With iodine; acetic acid; In ethanol;

DOI:10.1134/S1070428011070165

upstream raw materials:

6-bis(prop-2-en-1-yl)amino-1-phenyl-1H-pyrazolo[3,4-d]-pyrimidin-4(5H)-one

6-chloro-1-phenyl-1,5-dihydro-4H-pyrazolo[3,4-d]pyrimidin-4-one

diallylamine

Downstream raw materials:

8-methylidene-1-phenyl-6-(prop-2-en-1-yl)-7,8-dihydro-1H-imidazo[1,2-a]-pyrazolo[4,3-e]pyrimidin-4(6H)-one

8-methyl-1-phenyl-6-(prop-2-en-1-yl)-1H-imidazo[1,2-a]pyrazolo[4,3-e]pyrimidin-4(5H)-one

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