trans-decahydro-5α-<(2,5-dimethoxyphenyl)methyl>-5β,6β,8aβ-trimethyl-1-naphthalenol

Base Information

Chemical Name:trans-decahydro-5α-<(2,5-dimethoxyphenyl)methyl>-5β,6β,8aβ-trimethyl-1-naphthalenol
CAS No.:80765-06-6
Molecular Formula:C₂₂H₃₄O₃
Molecular Weight:346.51
Hs Code.:

Synonyms:trans-decahydro-5α-<(2,5-dimethoxyphenyl)methyl>-5β,6β,8aβ-trimethyl-1-naphthalenol

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Chemical Property of trans-decahydro-5α-<(2,5-dimethoxyphenyl)methyl>-5β,6β,8aβ-trimethyl-1-naphthalenol

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Technology Process of trans-decahydro-5α-<(2,5-dimethoxyphenyl)methyl>-5β,6β,8aβ-trimethyl-1-naphthalenol

There total 8 articles about trans-decahydro-5α-<(2,5-dimethoxyphenyl)methyl>-5β,6β,8aβ-trimethyl-1-naphthalenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 80765-04-4
trans-decahydro-5α-<(2,5-dimethoxyphenyl)methyl>-5β,8aβ-dimethyl-6-methylene-1-naphthalenol

: 80765-06-6
(1S,4aS,5R,6R,8aS)-5-(2,5-Dimethoxy-benzyl)-5,6,8a-trimethyl-decahydro-naphthalen-1-ol

: 80765-06-6
trans-decahydro-5α-<(2,5-dimethoxyphenyl)methyl>-5β,6β,8aβ-trimethyl-1-naphthalenol

Guidance literature:: With methanol; hydrogen; palladium on activated charcoal; In triethylamine; at 30 ℃; for 6h; under 760 Torr; Yields of byproduct given;
DOI:10.1021/jo00348a025

Reference yield: 80.0%

: 80765-04-4
trans-decahydro-5α-<(2,5-dimethoxyphenyl)methyl>-5β,8aβ-dimethyl-6-methylene-1-naphthalenol

: 80765-06-6
(1S,4aS,5R,6R,8aS)-5-(2,5-Dimethoxy-benzyl)-5,6,8a-trimethyl-decahydro-naphthalen-1-ol

: 80765-06-6
trans-decahydro-5α-<(2,5-dimethoxyphenyl)methyl>-5β,6β,8aβ-trimethyl-1-naphthalenol

Guidance literature:: With methanol; hydrogen; palladium on activated charcoal; In triethylamine; at 30 ℃; for 6h; under 760 Torr; Yields of byproduct given;
DOI:10.1021/jo00348a025

Reference yield:

: 60732-17-4
2,5-dimethoxybenzyl bromide

: 80765-06-6
(1S,4aS,5R,6R,8aS)-5-(2,5-Dimethoxy-benzyl)-5,6,8a-trimethyl-decahydro-naphthalen-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Li / 1.) NH₃ (liquid), THF, 0.5 h, 2.) 15 min

2: 85 percent / dimethylsulfoxide / 40 h / 75 - 80 °C

3: H₂, methanol / 10percent Pd/C / triethylamine / 6 h / 30 °C / 760 Torr

With methanol; hydrogen; lithium; palladium on activated charcoal; In dimethyl sulfoxide; triethylamine;
DOI:10.1021/jo00348a025