(2-oxo-1,3-dioxolan-4-yl)methyl 3-methoxy-4-((2-oxo-1,3-dioxolan-4-yl)methoxy) benzoate

Base Information

Chemical Name:(2-oxo-1,3-dioxolan-4-yl)methyl 3-methoxy-4-((2-oxo-1,3-dioxolan-4-yl)methoxy) benzoate
CAS No.:1584677-16-6
Molecular Formula:C₁₆H₁₆O₁₀
Molecular Weight:368.297
Hs Code.:

Synonyms:(2-oxo-1,3-dioxolan-4-yl)methyl 3-methoxy-4-((2-oxo-1,3-dioxolan-4-yl)methoxy) benzoate

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Chemical Property of (2-oxo-1,3-dioxolan-4-yl)methyl 3-methoxy-4-((2-oxo-1,3-dioxolan-4-yl)methoxy) benzoate

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Technology Process of (2-oxo-1,3-dioxolan-4-yl)methyl 3-methoxy-4-((2-oxo-1,3-dioxolan-4-yl)methoxy) benzoate

There total 2 articles about (2-oxo-1,3-dioxolan-4-yl)methyl 3-methoxy-4-((2-oxo-1,3-dioxolan-4-yl)methoxy) benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 124-38-9,18923-20-1
carbon dioxide

: 1393710-63-8
oxiran-2-ylmethyl 3-methoxy-4-(oxiran-2-ylmethoxy)benzoate

: 1584677-16-6
(2-oxo-1,3-dioxolan-4-yl)methyl 3-methoxy-4-((2-oxo-1,3-dioxolan-4-yl)methoxy) benzoate

Guidance literature:: With lithium bromide; In acetone; at 80 ℃; for 12h; under 9000.9 Torr; Autoclave;
DOI:10.1039/c3gc42613k

Reference yield:

: 121-34-6
3-methoxy-4-hydroxybenzoic acid

: 1584677-16-6
(2-oxo-1,3-dioxolan-4-yl)methyl 3-methoxy-4-((2-oxo-1,3-dioxolan-4-yl)methoxy) benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-benzyl-N,N,N-triethylammonium chloride / 1 h / 80 °C

1.2: 0.5 h / 20 °C

2.1: lithium bromide / acetone / 12 h / 80 °C / 9000.9 Torr / Autoclave

With N-benzyl-N,N,N-triethylammonium chloride; lithium bromide; In acetone;
DOI:10.1039/c3gc42613k