4-(2-furanoyl)-1,2,3,4-tetrahydro-4-phenyl-1-pivaloyl-2-quinolinol

Base Information

Chemical Name:4-(2-furanoyl)-1,2,3,4-tetrahydro-4-phenyl-1-pivaloyl-2-quinolinol
CAS No.:87091-20-1
Molecular Formula:C₂₅H₂₅NO₄
Molecular Weight:403.478
Hs Code.:

Synonyms:4-(2-furanoyl)-1,2,3,4-tetrahydro-4-phenyl-1-pivaloyl-2-quinolinol

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Chemical Property of 4-(2-furanoyl)-1,2,3,4-tetrahydro-4-phenyl-1-pivaloyl-2-quinolinol

Chemical Property:

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Technology Process of 4-(2-furanoyl)-1,2,3,4-tetrahydro-4-phenyl-1-pivaloyl-2-quinolinol

There total 6 articles about 4-(2-furanoyl)-1,2,3,4-tetrahydro-4-phenyl-1-pivaloyl-2-quinolinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 87091-11-0
1-(2-furanoyl)-2-phenyl-2-(pivaloylamidophenyl)pent-4-en-1-one

: 87091-20-1
4-(2-furanoyl)-1,2,3,4-tetrahydro-4-phenyl-1-pivaloyl-2-quinolinol

Guidance literature:: With sodium periodate; osmium(VIII) oxide; In diethyl ether; for 19h; Ambient temperature;

Reference yield:

: 98-01-1
furfural

: 87091-20-1
4-(2-furanoyl)-1,2,3,4-tetrahydro-4-phenyl-1-pivaloyl-2-quinolinol

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / n-BuLi, TMEDA / tetrahydrofuran; hexane / -30 °C

2: 1) DMSO, trifluoroacetic anhydride, 2) triethylamine / 1) dichloromethane, -65 - -60 deg C, 30 min, 2) dichloromethane, -60 deg C, 5 min

3: 99 percent / sodium hydroxide, tetra-n-butylamonium bromide / CH₂Cl₂; H₂O / 18 h / 23 °C

4: 86 percent / 1,3,5-trimethyl-benzene / 3.5 h / 165 °C

5: 91 percent / osmium tetroxide, sodium periodate / diethyl ether / 19 h / Ambient temperature

With sodium hydroxide; sodium periodate; osmium(VIII) oxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; tetrabutylammomium bromide; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; 1,3,5-trimethyl-benzene;

Reference yield:

: 85864-33-1
phenyl(2-pivaloylamidophenyl)methane

: 87091-20-1
4-(2-furanoyl)-1,2,3,4-tetrahydro-4-phenyl-1-pivaloyl-2-quinolinol

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / n-BuLi, TMEDA / tetrahydrofuran; hexane / -30 °C

2: 1) DMSO, trifluoroacetic anhydride, 2) triethylamine / 1) dichloromethane, -65 - -60 deg C, 30 min, 2) dichloromethane, -60 deg C, 5 min

3: 99 percent / sodium hydroxide, tetra-n-butylamonium bromide / CH₂Cl₂; H₂O / 18 h / 23 °C

4: 86 percent / 1,3,5-trimethyl-benzene / 3.5 h / 165 °C

5: 91 percent / osmium tetroxide, sodium periodate / diethyl ether / 19 h / Ambient temperature

With sodium hydroxide; sodium periodate; osmium(VIII) oxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; tetrabutylammomium bromide; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; 1,3,5-trimethyl-benzene;