2,4-diamino-5-<3,5-dimethoxy-4-<3-(3'-methyl-4'-(4''-nitrophenyl)sulfonylanilino)propoxy>benzyl>pyrimidine

Base Information

Chemical Name:2,4-diamino-5-<3,5-dimethoxy-4-<3-(3'-methyl-4'-(4''-nitrophenyl)sulfonylanilino)propoxy>benzyl>pyrimidine
CAS No.:176512-49-5
Molecular Formula:C₂₉H₃₂N₆O₇S
Molecular Weight:608.675
Hs Code.:

Synonyms:2,4-diamino-5-<3,5-dimethoxy-4-<3-(3'-methyl-4'-(4''-nitrophenyl)sulfonylanilino)propoxy>benzyl>pyrimidine

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Chemical Property of 2,4-diamino-5-<3,5-dimethoxy-4-<3-(3'-methyl-4'-(4''-nitrophenyl)sulfonylanilino)propoxy>benzyl>pyrimidine

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Technology Process of 2,4-diamino-5-<3,5-dimethoxy-4-<3-(3'-methyl-4'-(4''-nitrophenyl)sulfonylanilino)propoxy>benzyl>pyrimidine

There total 5 articles about 2,4-diamino-5-<3,5-dimethoxy-4-<3-(3'-methyl-4'-(4''-nitrophenyl)sulfonylanilino)propoxy>benzyl>pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 21253-58-7
2,4-diamino-5-(3,5-dimethoxy-4-hydroxybenzyl)pyrimidine

: 176512-45-1
(3-Bromo-propyl)-[3-methyl-4-(4-nitro-benzenesulfonyl)-phenyl]-amine

: 176512-49-5
2,4-diamino-5-<3,5-dimethoxy-4-<3-(3'-methyl-4'-(4''-nitrophenyl)sulfonylanilino)propoxy>benzyl>pyrimidine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1002/ardp.19963290309

Reference yield:

: 176512-23-5
3-methyl-4-(4-nitrophenylthio)aniline

: 176512-49-5
2,4-diamino-5-<3,5-dimethoxy-4-<3-(3'-methyl-4'-(4''-nitrophenyl)sulfonylanilino)propoxy>benzyl>pyrimidine

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 3 h

2: 74 percent / NaI, CuI, aq. KOH / ethanol / Heating

3: 92 percent / 30percent H₂O₂ / acetic acid / 65 °C

4: 89 percent / conc. H₂SO₄

5: 24 percent / K₂CO₃ / dimethylformamide / Ambient temperature

With potassium hydroxide; copper(l) iodide; sulfuric acid; dihydrogen peroxide; potassium carbonate; sodium iodide; In pyridine; ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/ardp.19963290309

Reference yield:

: 176512-26-8
4-Methyl-N-[3-methyl-4-(4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

: 176512-49-5
2,4-diamino-5-<3,5-dimethoxy-4-<3-(3'-methyl-4'-(4''-nitrophenyl)sulfonylanilino)propoxy>benzyl>pyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / NaI, CuI, aq. KOH / ethanol / Heating

2: 92 percent / 30percent H₂O₂ / acetic acid / 65 °C

3: 89 percent / conc. H₂SO₄

4: 24 percent / K₂CO₃ / dimethylformamide / Ambient temperature

With potassium hydroxide; copper(l) iodide; sulfuric acid; dihydrogen peroxide; potassium carbonate; sodium iodide; In ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/ardp.19963290309