2-(N,N-Dibenzylamino)ethyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

Base Information

Chemical Name:2-(N,N-Dibenzylamino)ethyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate
CAS No.:143746-13-8
Molecular Formula:C₂₄H₃₂N₂O₃
Molecular Weight:396.53
Hs Code.:

Synonyms:2-(N,N-Dibenzylamino)ethyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

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Chemical Property of 2-(N,N-Dibenzylamino)ethyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

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Technology Process of 2-(N,N-Dibenzylamino)ethyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

There total 3 articles about 2-(N,N-Dibenzylamino)ethyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 101-06-4
N,N-dibenzyl-2-aminoethanol

: 146176-60-5
2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl chloride

: 143746-13-8
2-(N,N-Dibenzylamino)ethyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

Guidance literature:: N,N-dibenzyl-2-aminoethanol; With sodium hydride; In tetrahydrofuran; for 1h; Heating;

2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl chloride; In tetrahydrofuran; for 6h; Heating;
DOI:10.1055/s-1999-3575

Reference yield:

: cyclohexyl-1-1,2-ethanediol

: 101-06-4
N,N-dibenzyl-2-aminoethanol

: 143746-13-8
2-(N,N-Dibenzylamino)ethyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

Guidance literature:: In 1,2-dimethoxyethane; water; mineral oil;

Reference yield:

: 100-44-7
benzyl chloride

: 143746-13-8
2-(N,N-Dibenzylamino)ethyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: K₂CO₃; NaOH / aq. methanol / 0.5 h / Heating

1.2: 43 percent / aq. methanol / 6 h / Heating

2.1: NaH / tetrahydrofuran / 1 h / Heating

2.2: 91 percent / tetrahydrofuran / 6 h / Heating

With sodium hydroxide; sodium hydride; potassium carbonate; In tetrahydrofuran; methanol; 1.1: Metallation / 1.2: Alkylation / 2.1: Metallation / 2.2: Acylation;
DOI:10.1055/s-1999-3575