Technology Process of C28H40Cl2N2O4
There total 12 articles about C28H40Cl2N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 45 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: sodium hydroxide / tetrabutylammomium bromide / water / 5 h / 20 °C
2: cetyltributylphosphonium bromide / N,N-dimethyl-formamide / 3 h / 75 °C
3: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C / 2070.21 Torr
4: triethylamine / dichloromethane / 20 °C
5: N-ethyl-N,N-diisopropylamine / 16 h / 45 °C
6: hydrazine / ethanol / 72 h / 20 °C
7: potassium carbonate / 1,4-dioxane / 16 h / 105 °C
8: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 45 °C
With
sodium hydroxide; tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; hydrazine;
palladium 10% on activated carbon; tetrabutylammomium bromide; cetyltributylphosphonium bromide;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: cetyltributylphosphonium bromide / N,N-dimethyl-formamide / 3 h / 75 °C
2: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C / 2070.21 Torr
3: triethylamine / dichloromethane / 20 °C
4: N-ethyl-N,N-diisopropylamine / 16 h / 45 °C
5: hydrazine / ethanol / 72 h / 20 °C
6: potassium carbonate / 1,4-dioxane / 16 h / 105 °C
7: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 45 °C
With
tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; hydrazine;
palladium 10% on activated carbon; cetyltributylphosphonium bromide;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;