C₃₂H₂₇N₇O₉

Base Information

Chemical Name:C₃₂H₂₇N₇O₉
CAS No.:1618636-79-5
Molecular Formula:C₃₂H₂₇N₇O₉
Molecular Weight:653.608
Hs Code.:

C<sub>32</sub>H<sub>27</sub>N<sub>7</sub>O<sub>9</sub>

Synonyms:C₃₂H₂₇N₇O₉

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Chemical Property of C₃₂H₂₇N₇O₉

Chemical Property:

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Technology Process of C₃₂H₂₇N₇O₉

There total 10 articles about C₃₂H₂₇N₇O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1618636-78-4
C₂₅H₂₄N₆O₅

: 7693-46-1
4-Nitrophenyl chloroformate

: 1618636-79-5
C₃₂H₂₇N₇O₉

Guidance literature:: With pyridine; In dichloromethane; acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1039/c4ob00923a

Reference yield:

: 108-67-8
1,3,5-trimethyl-benzene

: 1618636-79-5
C₃₂H₂₇N₇O₉

Guidance literature:: Multi-step reaction with 11 steps

1: sulfuric acid; nitric acid / 0.33 h

2: chromium(VI) oxide; acetic acid / Reflux

3: sulfuric acid / Reflux

4: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Reflux

5: silver(II) sulfate / water / 3 h / Reflux

6: zinc; acetic acid / dichloromethane; acetonitrile / 5 h / 20 °C

7: hydrogenchloride; sodium nitrite; sodium azide / water / 20 °C / Reflux

8: 1H-imidazole / dichloromethane / 3 h / 20 °C

9: dicyclohexyl-carbodiimide; dmap / dichloromethane / 0 °C / Inert atmosphere

10: tetrabutyl ammonium fluoride / dichloromethane / 5 h / 20 °C

11: pyridine / dichloromethane; acetonitrile / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; hydrogenchloride; dmap; N-Bromosuccinimide; sodium azide; silver(II) sulfate; 2,2'-azobis(isobutyronitrile); sulfuric acid; tetrabutyl ammonium fluoride; nitric acid; chromium(VI) oxide; acetic acid; dicyclohexyl-carbodiimide; zinc; sodium nitrite; In tetrachloromethane; dichloromethane; water; acetonitrile;
DOI:10.1039/c4ob00923a

Reference yield:

: 603-71-4,34505-32-3,82795-90-2
nitromesitylene

: 1618636-79-5
C₃₂H₂₇N₇O₉

Guidance literature:: Multi-step reaction with 10 steps

1: chromium(VI) oxide; acetic acid / Reflux

2: sulfuric acid / Reflux

3: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Reflux

4: silver(II) sulfate / water / 3 h / Reflux

5: zinc; acetic acid / dichloromethane; acetonitrile / 5 h / 20 °C

6: hydrogenchloride; sodium nitrite; sodium azide / water / 20 °C / Reflux

7: 1H-imidazole / dichloromethane / 3 h / 20 °C

8: dicyclohexyl-carbodiimide; dmap / dichloromethane / 0 °C / Inert atmosphere

9: tetrabutyl ammonium fluoride / dichloromethane / 5 h / 20 °C

10: pyridine / dichloromethane; acetonitrile / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; hydrogenchloride; dmap; N-Bromosuccinimide; sodium azide; silver(II) sulfate; 2,2'-azobis(isobutyronitrile); sulfuric acid; tetrabutyl ammonium fluoride; chromium(VI) oxide; acetic acid; dicyclohexyl-carbodiimide; zinc; sodium nitrite; In tetrachloromethane; dichloromethane; water; acetonitrile;
DOI:10.1039/c4ob00923a