Technology Process of C36H31N5O2
There total 3 articles about C36H31N5O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C28H24N4O;
With
triethylamine;
In
dichloromethane;
at 0 ℃;
for 0.166667h;
N-hydroxy-4-methylbenzenecarboximidoyl chloride;
In
dichloromethane;
at 0 - 20 ℃;
for 10h;
DOI:10.1021/ja4066656
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: copper(l) chloride; (S,S)-2,6-bis(4-phenyl-2-oxazolinyl)pyridine / 0.5 h / 0 °C
1.2: 96 h / 0 °C
2.1: triethylamine / dichloromethane / 0.17 h / 0 °C
2.2: 10 h / 0 - 20 °C
With
triethylamine; copper(l) chloride; (S,S)-2,6-bis(4-phenyl-2-oxazolinyl)pyridine;
In
dichloromethane;
DOI:10.1021/ja4066656
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / acetonitrile / 6 h / 70 °C
2.1: copper(l) chloride; (S,S)-2,6-bis(4-phenyl-2-oxazolinyl)pyridine / 0.5 h / 0 °C
2.2: 96 h / 0 °C
3.1: triethylamine / dichloromethane / 0.17 h / 0 °C
3.2: 10 h / 0 - 20 °C
With
tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; triethylamine; copper(l) chloride; (S,S)-2,6-bis(4-phenyl-2-oxazolinyl)pyridine;
In
dichloromethane; acetonitrile;
DOI:10.1021/ja4066656