N-[(Z)-[cyclopropyl(phenyl)methylidene]amino]-2,4-dinitroaniline

Base Information

Chemical Name:N-[(Z)-[cyclopropyl(phenyl)methylidene]amino]-2,4-dinitroaniline
CAS No.:75343-45-2
Molecular Formula:C16H14 N4 O4
Molecular Weight:326.312
Hs Code.:
NSC Number:230219
DSSTox Substance ID:DTXSID00429631

Synonyms:NSC230219;75343-45-2;DTXSID00429631;NSC-230219

Suppliers and Price of N-[(Z)-[cyclopropyl(phenyl)methylidene]amino]-2,4-dinitroaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of N-[(Z)-[cyclopropyl(phenyl)methylidene]amino]-2,4-dinitroaniline

Chemical Property:

Vapor Pressure:9E-10mmHg at 25°C
Boiling Point:490.6°Cat760mmHg
Flash Point:250.5°C
Density:1.45g/cm³
XLogP3:5.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:326.10150494
Heavy Atom Count:24
Complexity:503

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC1C(=NNC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-])C3=CC=CC=C3
Isomeric SMILES:C1CC1/C(=N/NC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-])/C3=CC=CC=C3

Technology Process of N-[(Z)-[cyclopropyl(phenyl)methylidene]amino]-2,4-dinitroaniline

There total 3 articles about N-[(Z)-[cyclopropyl(phenyl)methylidene]amino]-2,4-dinitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1007-03-0
1-phenyl-1-cyclopropylmethanol

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 75343-45-2
cyclopropyl-phenyl ketone-(2,4-dinitro-phenylhydrazone)

Guidance literature:: 1-phenyl-1-cyclopropylmethanol; With peracetic acid; C₉H₁₇NO₅S^(1-)*C₁₁H₁₂IN₂⁽¹⁺⁾; acetic acid; In 1,1,1,3',3',3'-hexafluoro-propanol; at 20 ℃; for 12h;

(2,4-dinitro-phenyl)-hydrazine; With sulfuric acid; In diethyl ether; ethanol; water;
DOI:10.1016/j.tetlet.2012.01.053

Reference yield:

: 3481-02-5
cyclopropyl phenyl ketone

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 75343-45-2
cyclopropyl-phenyl ketone-(2,4-dinitro-phenylhydrazone)

Guidance literature:: DOI:10.1021/ja01122a070

Reference yield:

: 74-85-1
ethene

: 4023-34-1
cyclopropanecarboxylic acid chloride

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 136120-61-1
1-cyclopropyl-3-phenyl-1-propanone 2,4-dinitrophenylhydrazone

: 75343-45-2
cyclopropyl-phenyl ketone-(2,4-dinitro-phenylhydrazone)

Guidance literature:: With aluminium trichloride; sulfuric acid; Yield given. Multistep reaction. Yields of byproduct given; 1a) CH₂Cl₂, 60 min, 1b) benzene, 3 h, 2) MeOH, 20 min;
DOI:10.1016/S0040-4020(01)80962-5