(1-(4-chlorophenyl)benzo[d]pyrrolo[2,1-b]thiazole-2,3-diyl)bis(methylene)bis(ethyl-carbamate)

Base Information

Chemical Name:(1-(4-chlorophenyl)benzo[d]pyrrolo[2,1-b]thiazole-2,3-diyl)bis(methylene)bis(ethyl-carbamate)
CAS No.:1383256-34-5
Molecular Formula:C₂₄H₂₄ClN₃O₄S
Molecular Weight:485.991
Hs Code.:

Synonyms:(1-(4-chlorophenyl)benzo[d]pyrrolo[2,1-b]thiazole-2,3-diyl)bis(methylene)bis(ethyl-carbamate)

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Chemical Property of (1-(4-chlorophenyl)benzo[d]pyrrolo[2,1-b]thiazole-2,3-diyl)bis(methylene)bis(ethyl-carbamate)

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Technology Process of (1-(4-chlorophenyl)benzo[d]pyrrolo[2,1-b]thiazole-2,3-diyl)bis(methylene)bis(ethyl-carbamate)

There total 5 articles about (1-(4-chlorophenyl)benzo[d]pyrrolo[2,1-b]thiazole-2,3-diyl)bis(methylene)bis(ethyl-carbamate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1383256-24-3
[1-(4-chlorophenyl)benzo[d]pyrrolo[2,1-b]thiazole-2,3-diyl]dimethanol

: 109-90-0
ethyl isocyanate

: 1383256-34-5
(1-(4-chlorophenyl)benzo[d]pyrrolo[2,1-b]thiazole-2,3-diyl)bis(methylene)bis(ethyl-carbamate)

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2012.03.030

Reference yield:

: 95-16-9
1,3-Benzothiazole

: 1383256-34-5
(1-(4-chlorophenyl)benzo[d]pyrrolo[2,1-b]thiazole-2,3-diyl)bis(methylene)bis(ethyl-carbamate)

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / dichloromethane / 17 h / 20 °C / Inert atmosphere

2.1: tetrafluoroboric acid / dichloromethane / 3 h / 20 °C

2.2: 13 h / 35 °C

3.1: lithium aluminium tetrahydride / diethyl ether; dichloromethane / 0.33 h / -5 - 0 °C

3.2: -5 - 0 °C

4.1: triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

With aluminum (III) chloride; lithium aluminium tetrahydride; tetrafluoroboric acid; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.ejmech.2012.03.030

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 1383256-34-5
(1-(4-chlorophenyl)benzo[d]pyrrolo[2,1-b]thiazole-2,3-diyl)bis(methylene)bis(ethyl-carbamate)

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / dichloromethane / 17 h / 20 °C / Inert atmosphere

2.1: tetrafluoroboric acid / dichloromethane / 3 h / 20 °C

2.2: 13 h / 35 °C

3.1: lithium aluminium tetrahydride / diethyl ether; dichloromethane / 0.33 h / -5 - 0 °C

3.2: -5 - 0 °C

4.1: triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

With aluminum (III) chloride; lithium aluminium tetrahydride; tetrafluoroboric acid; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.ejmech.2012.03.030