Methyl 5-cyclohexyl-3-methyl-5-oxo-2-pentenoate

Base Information

Chemical Name:Methyl 5-cyclohexyl-3-methyl-5-oxo-2-pentenoate
CAS No.:14619-59-1
Molecular Formula:C₁₃H₂₀O₃
Molecular Weight:224.3
Hs Code.:
European Community (EC) Number:604-515-7
DSSTox Substance ID:DTXSID50234914,DTXSID401241904

Synonyms:DTXSID50234914;DTXSID401241904;Methyl 5-cyclohexyl-3-methyl-5-oxo-2-pentenoate;14619-59-1

Suppliers and Price of Methyl 5-cyclohexyl-3-methyl-5-oxo-2-pentenoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Methyl 5-cyclohexyl-3-methyl-5-oxo-2-pentenoate

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:224.14124450
Heavy Atom Count:16
Complexity:286

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CC(=O)OC)CC(=O)C1CCCCC1

Technology Process of Methyl 5-cyclohexyl-3-methyl-5-oxo-2-pentenoate

There total 4 articles about Methyl 5-cyclohexyl-3-methyl-5-oxo-2-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 924-50-5
Methyl 3,3-dimethylacrylate

: 2719-27-9
cyclohexanylcarbonyl chloride

: 14619-60-4
methyl 5-oxo-3-methyl-5-cyclohexyl-3-pentenoate

: 14619-59-1
3-Methyl-5-cyclohexyl-5-oxo-penten-⁽²⁾-saeure-⁽¹⁾-methylester

Guidance literature:: With aluminum (III) chloride; In dichloromethane; for 3h; Reflux;

Reference yield:

: 541-47-9
3-Methylbutenoic acid

: 14619-60-4
methyl 5-oxo-3-methyl-5-cyclohexyl-3-pentenoate

: 14619-59-1
3-Methyl-5-cyclohexyl-5-oxo-penten-⁽²⁾-saeure-⁽¹⁾-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 5 h / Reflux

2: aluminum (III) chloride / dichloromethane / 3 h / Reflux

With aluminum (III) chloride; sulfuric acid; In dichloromethane;

Reference yield:

: 98-89-5
Cyclohexanecarboxylic acid

: 14619-60-4
methyl 5-oxo-3-methyl-5-cyclohexyl-3-pentenoate

: 14619-59-1
3-Methyl-5-cyclohexyl-5-oxo-penten-⁽²⁾-saeure-⁽¹⁾-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; thionyl chloride / 3 h / Reflux

2: aluminum (III) chloride / dichloromethane / 3 h / Reflux

With pyridine; aluminum (III) chloride; thionyl chloride; In dichloromethane;