C₁₆H₁₉BrClNO₃

Base Information

Chemical Name:C₁₆H₁₉BrClNO₃
CAS No.:1583253-13-7
Molecular Formula:C₁₆H₁₉BrClNO₃
Molecular Weight:388.689
Hs Code.:

C<sub>16</sub>H<sub>19</sub>BrClNO<sub>3</sub>

Synonyms:C₁₆H₁₉BrClNO₃

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Chemical Property of C₁₆H₁₉BrClNO₃

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Technology Process of C₁₆H₁₉BrClNO₃

There total 5 articles about C₁₆H₁₉BrClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1583253-12-6
C₇H₁₂BrClO

: 49647-20-3
4-acetylphenyl isocyanate

: 1583253-13-7
C₁₆H₁₉BrClNO₃

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ja5013307

Reference yield:

: 1191268-97-9
C₂₃H₂₉ClOSi

: 1583253-13-7
C₁₆H₁₉BrClNO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine hydrogenfluoride; pyridine / acetonitrile / 10 h / 0 - 20 °C

2.1: pyridine; dmap / dichloromethane / 5 h / 0 - 20 °C

3.1: B-Br-9-BBN / dichloromethane / 7 h / 0 °C

3.2: 0.83 h / 20 °C

4.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

5.1: dmap / dichloromethane / 1 h / 20 °C

With pyridine; B-Br-9-BBN; dmap; diisobutylaluminium hydride; pyridine hydrogenfluoride; In dichloromethane; toluene; acetonitrile;
DOI:10.1021/ja5013307

Reference yield:

: 1583253-09-1
C₇H₁₁ClO

: 1583253-13-7
C₁₆H₁₉BrClNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine; dmap / dichloromethane / 5 h / 0 - 20 °C

2.1: B-Br-9-BBN / dichloromethane / 7 h / 0 °C

2.2: 0.83 h / 20 °C

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

4.1: dmap / dichloromethane / 1 h / 20 °C

With pyridine; B-Br-9-BBN; dmap; diisobutylaluminium hydride; In dichloromethane; toluene;
DOI:10.1021/ja5013307