C₂₇H₄₃BrN₂O₇Si

Base Information

Chemical Name:C₂₇H₄₃BrN₂O₇Si
CAS No.:1357622-59-3
Molecular Formula:C₂₇H₄₃BrN₂O₇Si
Molecular Weight:615.637
Hs Code.:

C<sub>27</sub>H<sub>43</sub>BrN<sub>2</sub>O<sub>7</sub>Si

Synonyms:C₂₇H₄₃BrN₂O₇Si

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Chemical Property of C₂₇H₄₃BrN₂O₇Si

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Technology Process of C₂₇H₄₃BrN₂O₇Si

There total 17 articles about C₂₇H₄₃BrN₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1357622-38-8
(R)-1-(tert-butyl)dimethylsilyloxy-2-((3-bromophenoxy)methyl)-3-isocyanopropane

: 625-45-6
2-methoxyacetic acid

: (3aS,6aR)-2,2-Dimethyl-4,6a-dihydro-3aH-[1,3]dioxolo[4,5-c]pyrrole

: 1357622-59-3
C₂₇H₄₃BrN₂O₇Si

Guidance literature:: In methanol; at 20 ℃; for 48h; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1039/c1ob06632c

Reference yield:

: 55904-12-6
((4R,5S)-5-Hydroxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methanol

: 1357622-59-3
C₂₇H₄₃BrN₂O₇Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: amano Porcine pancreas lipase / 20 h / 20 °C / Inert atmosphere; Enzymatic reaction

2.1: triethylamine / dichloromethane / -18 °C / Inert atmosphere

3.1: sodium azide / N,N-dimethyl-formamide / 42 h / 100 °C / Inert atmosphere

4.1: potassium hydroxide / methanol / 0.33 h / 0 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.17 h / -70 °C / Inert atmosphere

5.2: 1 h / -70 - -60 °C / Inert atmosphere

6.1: triphenylphosphine / tetrahydrofuran / 24 h / 50 °C / Inert atmosphere; Molecular sieve

7.1: methanol / 48 h / 20 °C / Inert atmosphere; Molecular sieve

With sodium azide; oxalyl dichloride; amano Porcine pancreas lipase; dimethyl sulfoxide; triethylamine; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 5.1: Swern oxidation / 5.2: Swern oxidation / 7.1: Ugi condensation;
DOI:10.1039/c1ob06632c

Reference yield:

: 1357623-31-4
C₇H₁₁N₃O₃

: 1357622-59-3
C₂₇H₄₃BrN₂O₇Si

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine / tetrahydrofuran / 24 h / 50 °C / Inert atmosphere; Molecular sieve

2: methanol / 48 h / 20 °C / Inert atmosphere; Molecular sieve

With triphenylphosphine; In tetrahydrofuran; methanol; 2: Ugi condensation;
DOI:10.1039/c1ob06632c