methyl 4,5-dihydro-4-oxo-2-phenylpyrrolo[1,2-a]quinoxaline-3-carboxylate

Base Information

• Chemical Name: methyl 4,5-dihydro-4-oxo-2-phenylpyrrolo[1,2-a]quinoxaline-3-carboxylate
• CAS No.: 1588870-69-2
• Molecular Formula: C₁₉H₁₄N₂O₃
• Molecular Weight: 318.332
• Mol file: 1588870-69-2.mol

Synonyms:methyl 4,5-dihydro-4-oxo-2-phenylpyrrolo[1,2-a]quinoxaline-3-carboxylate

Chemical Property of methyl 4,5-dihydro-4-oxo-2-phenylpyrrolo[1,2-a]quinoxaline-3-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 4,5-dihydro-4-oxo-2-phenylpyrrolo[1,2-a]quinoxaline-3-carboxylate

There total 2 articles about methyl 4,5-dihydro-4-oxo-2-phenylpyrrolo[1,2-a]quinoxaline-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

nitrostyrene (5153-67-3) + 1,2-diamino-benzene (95-54-5) + dimethyl acetylenedicarboxylate (762-42-5) → methyl 4,5-dihydro-4-oxo-2-phenylpyrrolo[1,2-a]quinoxaline-3-carboxylate (1588870-69-2)

Guidance literature:

With aminosulfonic acid; In acetonitrile; for 24h; Reflux;

DOI:10.1002/hlca.201300209

Reference yield: 82.0%

(2-nitroethenyl)benzene (102-96-5) + 1,2-diamino-benzene (95-54-5) + dimethyl acetylenedicarboxylate (762-42-5) → methyl 4,5-dihydro-4-oxo-2-phenylpyrrolo[1,2-a]quinoxaline-3-carboxylate (1588870-69-2)

Guidance literature:

1,2-diamino-benzene; dimethyl acetylenedicarboxylate; In acetonitrile; at 25 ℃; for 0.5h;

(2-nitroethenyl)benzene; With toluene-4-sulfonic acid; In acetonitrile; at 25 ℃;

DOI:10.2174/1386207316666131227150430

upstream raw materials:

(2-nitroethenyl)benzene

1,2-diamino-benzene

dimethyl acetylenedicarboxylate

nitrostyrene