6-O-triisopropylsilyl-3-O-triphenylsilyl glucal

Base Information

Chemical Name:6-O-triisopropylsilyl-3-O-triphenylsilyl glucal
CAS No.:322648-40-8
Molecular Formula:C₃₃H₄₄O₄Si₂
Molecular Weight:560.881
Hs Code.:

Synonyms:6-O-triisopropylsilyl-3-O-triphenylsilyl glucal

Suppliers and Price of 6-O-triisopropylsilyl-3-O-triphenylsilyl glucal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 6-O-triisopropylsilyl-3-O-triphenylsilyl glucal

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 6-O-triisopropylsilyl-3-O-triphenylsilyl glucal

There total 1 articles about 6-O-triisopropylsilyl-3-O-triphenylsilyl glucal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 76-86-8
Triphenylsilyl chloride

: 137915-37-8
1,2-dideoxy-6-O-triisopropylsilyl-D-arabino-1-hexenopyranose

: 322648-40-8
6-O-triisopropylsilyl-3-O-triphenylsilyl glucal

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/ja0022730

Reference yield:

: 127061-08-9
2,3,4-tri-O-benzyl-L-fucopyranosyl fluoride

: 322648-40-8
6-O-triisopropylsilyl-3-O-triphenylsilyl glucal

: (2R,3R,4R)-2-Triisopropylsilanyloxymethyl-4-triphenylsilanyloxy-3-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-3,4-dihydro-2H-pyran

Guidance literature:: With silver perchlorate; Di-tert-butylpyridine; tin(ll) chloride; In diethyl ether; at 20 ℃; for 22h;
DOI:10.1021/ja0022730

Reference yield:

: 322648-40-8
6-O-triisopropylsilyl-3-O-triphenylsilyl glucal

: 210427-06-8
(2R,3S,4R)-2-Triisopropylsilanyloxymethyl-3-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-3,4-dihydro-2H-pyran-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1: AgClO₄; di-tert-butylpyridine; 4A MS / SnCl₂ / diethyl ether / 22 h / 20 °C

2: K₂CO₃; MeOH / tetrahydrofuran / 20 h

With methanol; silver perchlorate; potassium carbonate; Di-tert-butylpyridine; tin(ll) chloride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja0022730